Synthesis and structure of 2,4,6-tris[tris(dimethylamino)silylamino]borazine:: {[(CH3)2N]3SiNH}3B3N3H3

被引:13
作者
Cheng, F [1 ]
Toury, B [1 ]
Archibald, SJ [1 ]
Bradley, JS [1 ]
机构
[1] Univ Hull, Dept Chem, Kingston Upon Hull HU6 7RX, N Humberside, England
基金
英国工程与自然科学研究理事会;
关键词
dimethylamino; silylamino; borazine; synthesis; structure;
D O I
10.1016/S0022-328X(02)01566-8
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
A novel compound 2,4,6-tris[tris(dimethylamino)silylamino]borazine {[(CH3)(2)N](3)SiNH}(3)B3N3H3 (1) was prepared by reaction between lithium tris(dimethylamino)silylamide [(CH3)(2)N](3)SiNHLi and 2,4,6-trichloroborazine Cl3B3N3H3. The molecular structure of 1 was discussed on the basis of its FTIR, NMR and X-ray crystallographic analysis. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:71 / 74
页数:4
相关论文
共 20 条
[1]  
BLICK KE, 1971, INORG CHEM, V10, P1133
[2]   B-TRICHLOROBORAZOLE [J].
BROWN, CA ;
LAUBENGAYER, AW .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1955, 77 (14) :3699-3700
[3]   THE STRUCTURE OF B-TRICHLOROBORAZOLE [J].
COURSEN, DL ;
HOARD, JL .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1952, 74 (07) :1742-1750
[5]   STRUCTURE OF BORAZINE [J].
HARSHBARGER, W ;
LEE, G ;
PORTER, RF ;
BAUER, SH .
INORGANIC CHEMISTRY, 1969, 8 (08) :1683-+
[6]   STRUCTURE OF B-MONOAMINOBORAZINE [J].
HARSHBARGER, W ;
LEE, GH ;
PORTER, RF ;
BAUER, SH .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1969, 91 (03) :551-+
[7]   STRUCTURE DETERMINATION ON BORON-NITROGEN COMPOUNDS .5. CRYSTAL AND MOLECULAR STRUCTURE OF B-TRIS(DIMETHYLAMINO)BORAZINE [J].
HESS, H ;
REISER, B .
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1971, 381 (01) :91-&
[8]   SYNTHESIS, CHARACTERIZATION, AND CONSOLIDATION OF SI3N4 OBTAINED FROM AMMONOLYSIS OF SICL4 [J].
MAZDIYASNI, KS ;
COOKE, CM .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1973, 56 (12) :628-633
[9]  
Rovai R, 1999, ANGEW CHEM INT EDIT, V38, P2036, DOI 10.1002/(SICI)1521-3773(19990712)38:13/14<2036::AID-ANIE2036>3.0.CO
[10]  
2-Q