Thermophysical properties by a pulse-heating reflectometric technique: Niobium, 1100 to 2700 K

被引:21
作者
Righini, F
Spisiak, J
Bussolino, GC
Gualano, M
机构
[1] CNR, Inst Metrol G Colonnetti, I-10135 Turin, Italy
[2] Slovak Acad Sci, Inst Phys, Bratislava, Slovakia
关键词
electrical resistivity; heat capacity; hemispherical total emissivity; high temperatures; niobium; pulse-heating; refractory metals;
D O I
10.1023/A:1022654804141
中图分类号
O414.1 [热力学];
学科分类号
摘要
Pulse-heating experiments were performed on niobium strips, taking the specimens from room temperature to the melting point is less than one second. The normal spectral emissivity of the strips was measured by integrating sphere I reflectometry, and, simultaneously, experimental data (radiance temperature. cur rent, voltage drop) for thermophysical properties were collected with submillisecond time resolution. The normal spectral emissivity results were used to compute the true temperature of the niobium strips; the heat capacity, electrical resistivity, and hemispherical total emissivity were evaluated in the temperature range 1100 to 2700 K. The results are compared with literature data obtained in pulse-heating experiments. It is concluded that combined measurements of normal spectral emissivity and of thermophysical properties on strip specimens provide results of the same quality as obtained using tubular specimens with a blackbody. The thermophysical property results on niobium also validate the normal spectral emissivity measurements by integrating sphere reflectometry.
引用
收藏
页码:1107 / 1116
页数:10
相关论文
共 15 条
[1]   HIGH-SPEED (SUBSECOND) MEASUREMENT OF HEAT-CAPACITY, ELECTRICAL RESISTIVITY, AND THERMAL-RADIATION PROPERTIES OF NIOBIUM IN RANGE 1500 TO 2700 K [J].
CEZAIRLIYAN, A .
JOURNAL OF RESEARCH OF THE NATIONAL BUREAU OF STANDARDS SECTION A-PHYSICS AND CHEMISTRY, 1971, A 75 (06) :565-+
[2]  
Cezairliyan A., 1972, High Temperatures - High Pressures, V4, P453
[3]  
*CIPM, 1981, BIPM P VERB COM INT, V49, P26
[4]  
*CIPM, 1986, BIPM P VERB COM INT, V54, P35
[5]  
IUPAC Commission on atomic weights, 1970, PURE APPL CHEM, V21, P91, DOI DOI 10.1351/PAC197021010091
[6]   SPECIFIC-HEAT AND ELECTRICAL-RESISTIVITY OF NIOBIUM MEASURED BY SUBSECOND CALORIMETRIC TECHNIQUE [J].
MAGLIC, KD ;
PEROVIC, NL ;
VUKOVIC, GS ;
ZEKOVIC, LP .
INTERNATIONAL JOURNAL OF THERMOPHYSICS, 1994, 15 (05) :963-972
[7]   THE INTERNATIONAL TEMPERATURE SCALE OF 1990 (ITS-90) [J].
PRESTONTHOMAS, H .
METROLOGIA, 1990, 27 (01) :3-10
[8]   Normal spectral emissivity of niobium (at 900 nm) by a pulse-heating reflectometric technique [J].
Righini, F ;
Spisiak, J ;
Bussolino, GC .
INTERNATIONAL JOURNAL OF THERMOPHYSICS, 1999, 20 (04) :1095-1106
[9]   MEASUREMENT OF THERMO-PHYSICAL PROPERTIES BY A PULSE-HEATING METHOD - NIOBIUM IN THE RANGE 1000-2500-K [J].
RIGHINI, F ;
ROBERTS, RB ;
ROSSO, A .
INTERNATIONAL JOURNAL OF THERMOPHYSICS, 1985, 6 (06) :681-693
[10]  
Righini F., 1997, High Temperatures - High Pressures, V29, P473, DOI 10.1068/htec281