Nanoscaled optical fibre obtained by the sol-gel process in the SiO2-ZrO2 system doped with rare earth ions

被引:22
作者
Brasse, G. [1 ]
Restoin, C. [1 ]
Auguste, J-L. [1 ]
Hautreux, S. [1 ]
Blondy, J-M. [1 ]
Iecomte, A. [2 ]
Sandoz, F. [3 ]
Pedrido, C. [3 ]
机构
[1] CNRS, Xlim Res Inst, UMR 6172, F-87060 Limoges, France
[2] CNRS, SPCTS, UMR 6638, F-87065 Limoges, France
[3] SILITEC FIBERS SA, CH-2017 Boudry, Switzerland
关键词
Sol-gel process; Optical fibre; Nanocrystals; Silica-zirconia xerogel; NANOSTRUCTURED MATERIALS; NANOCRYSTALS; GLASSES;
D O I
10.1016/j.optmat.2008.03.021
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A SiO2-ZrO2 nanostructured optical fibre is fabricated using the chemical sol-gel method associated to the drawing process; the structural and the waveguiding properties are studied. The refractive index difference (RIP) between the core and the cladding is 0.021 for a 30 mol% ZrO2 - 70 mol% SiO2 care composition. Illumination of the fibre with a supercontinuum source (350-1750 nm) shows that the light is guided over this entire range. The measured attenuation losses are 0.7 dB/m at a 1064 nm wavelength and the calculated cutoff wavelength is 714 nm, To control the nanostructure and the geometric parameters of the fibre, a preliminary study of the SiO2-ZrO2 binary system has been done, by X-ray diffraction (XRD), differential thermal analysis (DTA), thermo gravimetric analysis (TGA), transmission electron microscopy (TEM) and scanning electron microscopy (SEM); in addition the evolution of the sol viscosity with the time is studied. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:765 / 768
页数:4
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