TEM Study of twist boundaries and colony boundaries in (Bi,Pb)(2)Sr2Ca2CU3Ox silver-sheathed tapes

被引：19

作者：

Grindatto, DP ^{[1
]}

Hensel, B ^{[1
]}

Grasso, G ^{[1
]}

Nissen, HU ^{[1
]}

Flukiger, R ^{[1
]}

机构：

[1] UNIV GENEVA,DEPT PHYS MAT CONDENSEE,CH-1211 GENEVA 4,SWITZERLAND

来源：

PHYSICA C | 1996年 / 271卷 / 1-2期

关键词：

(Bi; Pb)(2)Sr2Ca2Cu3Ox; transmission electron microscopy (tem); grain boundaries; superconducting tape; critical current density;

D O I：

10.1016/S0921-4534(96)00517-5

中图分类号：

O59 [应用物理学];

学科分类号：

摘要：

The grain boundaries in high-j(c) (Bi,Pb)(2)Sr2Ca2Cu3Ox silver-sheathed tapes have been investigated using transmission electron microscopy, The typical microstructural feature in these tapes are the colonies, which consist of grains with a common c-axis. The grains within a colony are piled up along the common c-axis and are separated by [001] twist boundaries. It was found that the rotation angle of these twist boundaries takes several definite values. Colony boundaries are formed between colonies having slightly tilted c-axes with respect to each other and are virtually free from amorphous material and intergranular phases, Two basic types of colony boundaries have been observed: the small-angle c-axis tilt boundary and the edge-on c-axis tilt boundary, The weak bonds between the BiO double layers are responsible for the mica-like crystalline structure of Bi2Sr2Can-1CunOx and their importance concerning the formation of colony boundaries is discussed.

引用

页码：155 / 163

页数：9

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