Microstructure of severely deformed metals determined by X-ray peak profile analysis

被引:73
作者
Gubicza, J
Nam, NH
Balogh, L
Hellmig, RJ
Stolyarov, VV
Estrin, Y
Ungár, T
机构
[1] Eotvos Lorand Univ, Dept Gen Phys, H-1117 Budapest 1518, Hungary
[2] Eotvos Lorand Univ, Dept Solid State Phys, H-1117 Budapest 1518, Hungary
[3] Tech Univ Clausthal, Inst Mat Engn & Technol, Clausthal Zellerfeld, Germany
[4] Ufa State Aviat Tech Univ, Inst Phys Perspect Mat, Ufa, Russia
关键词
metals; dislocations; X-ray diffraction;
D O I
10.1016/j.jallcom.2003.11.162
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Two essentially different metals, fee copper and hexagonal titanium, were deformed by equal channel angular pressing (ECAP) up to eight passes. The microstructure developed as a result of severe plastic deformation (SPD) was studied by X-ray peak profile analysis. The formation of submicron grain sized structures was studied as a function of the number of ECAP passes. Thermal stability of the microstructure in both copper and titanium was examined by differential scanning calorimetry (DSC). During the isothermal heat-treatment of copper a bi-modal microstructure was formed, as manifested in a special shape of the peak profiles. In titanium, a considerable fraction of dislocations gets annihilated at temperatures well below the exothermic peak in the DSC curve. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:248 / 252
页数:5
相关论文
共 22 条
[1]   Calculation of deformation behavior and texture evolution during equal channel angular pressing of IF steel using dislocation based modeling of strain hardening [J].
Baik, SC ;
Estrin, Y ;
Kim, HS ;
Jeong, HT ;
Hellmig, RJ .
TEXTURES OF MATERIALS, PTS 1 AND 2, 2002, 408-4 :697-702
[2]   The high-strain-rate response of alpha-titanium: Experiments, deformation mechanisms and modeling [J].
Chichili, DR ;
Ramesh, KT ;
Hemker, KJ .
ACTA MATERIALIA, 1998, 46 (03) :1025-1043
[3]   Contrast factors of dislocations in the hexagonal crystal system [J].
Dragomir, IC ;
Ungár, T .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2002, 35 :556-564
[4]  
Girshick A, 1998, PHILOS MAG A, V77, P999, DOI 10.1080/01418619808221224
[5]  
HEARMON RFS, 1966, LANDOLTBORNSTEIN, V1, P1
[6]  
KRIVOGLAZ MA, 1996, THEORY XRAY THERMAL
[7]  
Kuzel R, 2004, DIFFRACTION ANALYSIS OF THE MICROSTRUCTURE OF MATERIALS, P229
[8]   X-RAY-DIFFRACTION LINE BROADENING DUE TO DISLOCATIONS IN NON-CUBIC MATERIALS .2. THE CASE OF ELASTIC-ANISOTROPY APPLIED TO HEXAGONAL CRYSTALS [J].
KUZEL, R ;
KLIMANEK, P .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1988, 21 :363-368
[9]   X-RAY-DIFFRACTION LINE BROADENING DUE TO DISLOCATIONS IN NON-CUBIC CRYSTALLINE MATERIALS .3. EXPERIMENTAL RESULTS FOR PLASTICALLY DEFORMED ZIRCONIUM [J].
KUZEL, R ;
KLIMANEK, P .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1989, 22 :299-307
[10]   Effect of a crystallite size distribution on X-ray diffraction line profiles and whole-powder-pattern fitting [J].
Langford, JI ;
Louër, D ;
Scardi, P .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2000, 33 (02) :964-974