Preparation of an Energetic-Energetic Cocrystal using Resonant Acoustic Mixing

被引:121
作者
Anderson, Stephen R. [1 ]
Ende, David J. Am [1 ]
Salan, Jerry S. [1 ]
Samuels, Philip [2 ]
机构
[1] Nalas Engn Serv Inc, Centerbrook, CT 06409 USA
[2] ARDEC, Picatinny Arsenal, NJ USA
关键词
LabRAM; Resonant acoustic mixing; Cocrystal; CL-20; HMX; Energetic cocrystal;
D O I
10.1002/prep.201400092
中图分类号
O69 [应用化学];
学科分类号
070301 [无机化学];
摘要
Resonant acoustic mixing (RAM) was applied to the preparation of an energetic-energetic cocrystal comprised of CL-20 and HMX in a 2:1mol ratio. We have prepared the cocrystal using the RAM technology in a resource-efficient manner providing near quantitative yield. The cocrystalline product from the RAM preparation is consistent with the product from solution crystallization.
引用
收藏
页码:637 / 640
页数:4
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