Determination of Cu, Fe, Pb and Zn by Flame-AAS after Preconcentration using Sodium Dodecyl Sulfate Coated Alumina Modified with Complexing Agent

被引：32

作者：

Ghaedi, Mehrorang ^{[1
]}

Niknam, Khodabakhsh ^{[2
]}

Shokrollahi, Ardeshir ^{[1
]}

Niknam, Ebrahim ^{[2
]}

机构：

[1] Univ Yasuj, Dept Chem, Yasuj 75914353, Iran

[2] Persian Gulf Univ, Dept Chem, Bushehr, Iran

来源：

JOURNAL OF THE CHINESE CHEMICAL SOCIETY | 2009年 / 56卷 / 01期

关键词：

Surfactant coated alumina; Atomic absorption spectrometry; Solid phase extraction; SOLID-PHASE EXTRACTION; ATOMIC-ABSORPTION-SPECTROMETRY; NATURAL-WATER SAMPLES; OPTICAL-EMISSION-SPECTROMETRY; HEAVY-METAL IONS; TRACE AMOUNTS; ACTIVATED CARBON; ENVIRONMENTAL-SAMPLES; WASTE-WATER; SPECTROPHOTOMETRIC DETERMINATION;

D O I：

10.1002/jccs.200900021

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A sensitive and simple method for the simultaneous preconcentration of trace transition and heavy metal ions is reported. The method is based on the adsorption of Cu, Fe, Pb and Zn on N,N'-Diacetyl-4-bromo-2,6-di(aminomethyl)anisole (DABDAMA) loaded on sodium dodecyl sulfate (SDS) coated alumina. The metal content on the complexes are eluted using 6 mL of 2 mol l(-1) nitric acid. The influences of the analytical parameters including pH and sample volume were investigated. The effects of matrix ions on the retentions of the analytes were also examined. The recoveries of analytes were generally higher than 95% with a low RSD. The method has been successfully applied for these metals content evaluation in samples including soil, blood and vegetable samples.

引用

收藏

页码：150 / 157

页数：8

相关论文

共 60 条

[1] Separation and preconcentration of silver ion using 2-mercaptobenzothiazole immobilized on surfactant-coated alumina [J].

Absalan, G ;

Mehrdjardi, MA .

SEPARATION AND PURIFICATION TECHNOLOGY, 2003, 33 (01) :95-101

[2] On-line preconcentration and determination of copper, lead and chromium(VI) using unloaded polyurethane foam packed column by flame atomic absorption spectrometry in natural waters and biological samples [J].

Anthemidis, AN ;

Zachariadis, GA ;

Stratis, JA .

TALANTA, 2002, 58 (05) :831-840

[3]

BUDHIRAJA RP, 2004, SEPARATION CHEM

[4] Determination of non-ionic polyethoxylated surfactants in wastewater and river water by mixed hemimicelle extraction and liquid chromatography-ion trap mass spectrometry [J].

Cantero, M ;

Rubio, S ;

Pérez-Bendito, D .

JOURNAL OF CHROMATOGRAPHY A, 2005, 1067 (1-2) :161-170

[5] Solid phase extraction of Cd, Cu, and Ni from leafy vegetables and plant leaves using amberlite XAD-2 functionalized with 2-hydroxy-acetophenone-thiosemicarbazone (HAPTSC) and determination by inductively coupled plasma atomic emission spectroscopy [J].

Chandra, GP ;

Seshaiah, K ;

Rao, YK ;

Wang, MC .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2006, 54 (08) :2868-2872

[6] Study on the solid phase extraction of Hg(II)-ABR chelate with C18 disks and its application to the determination of mercury in tobacco and tobacco additives [J].

Chen, ZY ;

Yang, GY ;

Hu, QF ;

Yin, JY ;

Su, QD .

JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2004, 51 (02) :297-302

[7] Application of total reflection X-ray fluorescence spectrometry in the textile industry [J].

Dogan, M ;

Soylak, M ;

Elçi, L ;

von Bohlen, A .

MIKROCHIMICA ACTA, 2002, 138 (1-2) :77-82

[8] Differential pulse polarographic determination of rhodium(III) and ruthenium(III) in synthetic samples after preconcentration of their quinolin-8-olate complexes onto microcrystalline naphthalene [J].

Dubey, RK ;

Bhalotra, A ;

Gupta, MK ;

Puri, BK .

MICROCHEMICAL JOURNAL, 1998, 58 (01) :117-126

[9] Speciation of Cr(III) and Cr(VI) in environmental samples after solid phase extraction on amberlite XAD-2000 [J].

Duran, Celal ;

Soylak, Mustafa ;

Bulut, Volkan Numan ;

Gundogdu, Ali ;

Tufekci, Mehmet ;

Elcid, Latif ;

Senturk, Hasan Basri .

JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2007, 54 (03) :625-634

[10] Preconcentration and separation of iron, zinc, cadmium and mercury, from waste water using Nile blue a grafted polyurethane foam [J].

El-shahat, MF ;

Moawed, EA ;

Zaid, MAA .

TALANTA, 2003, 59 (05) :851-866

← 1 2 3 4 5 6 →