Development of a real-time defocus image modulation processing electron microscope. I. Construction

被引:22
作者
Kimura, Y [1 ]
Takai, Y
Kawasaki, T
Shimizu, R
Ikuta, T
Isakozawa, S
Satou, Y
Ichihashi, M
机构
[1] Osaka Univ, Grad Sch Engn, Dept Appl Phys, Suita, Osaka 5650871, Japan
[2] Osaka Electrocommun Univ, Neyagawa, Osaka 5728530, Japan
[3] Hitachi Ltd, Instrument Div, Katsuta, Ibaraki 3120033, Japan
来源
JOURNAL OF ELECTRON MICROSCOPY | 1999年 / 48卷 / 06期
关键词
DIMP-EM; real-time aberration free observation; floating type high voltage power supply; defocus modulation; high voltage modulation; low capacitance double shielded HV-cable;
D O I
10.1093/oxfordjournals.jmicro.a023759
中图分类号
TH742 [显微镜];
学科分类号
摘要
A real-time 'defocus image modulation processing electron microscope' (DIMP-EM) has been developed by the 'Research for the Future Program' which was started in 1996 by the Japan Society for the Promotion of Science (JSPS). This real-time DIMP-EM produces images which are free of spherical aberration when working in either the phase contrast or amplitude contrast modes which are produced in real-time by actively modulating the accelerating voltage. For this microscope it was essential to develop a floating type, high voltage power supply system. The performance of this custom made, floating type 200 kV accelerating voltage system, and the spherical aberration free phase contrast image of a gold particle observed in real-time at 4/30 s are presented. This paper describes the DIMP-EM from two sides, namely, the technical side and application side. We describe the construction of the DIMP-EM in this paper, and the result of observation with DIMP-EM will be described in next paper.
引用
收藏
页码:873 / 878
页数:6
相关论文
共 8 条
[1]  
ANDO T, 1994, J ELECTRON MICROSC, V43, P10
[2]  
Ando T, 1997, OPTIK, V106, P147
[3]  
Ando T, 1997, OPTIK, V104, P163
[4]   DEVELOPMENT OF REAL-TIME DEFOCUS-MODULATION-TYPE ACTIVE IMAGE-PROCESSING (DMAIP) FOR SPHERICAL-ABERRATION-FREE TEM OBSERVATION [J].
ANDO, T ;
TANIGUCHI, Y ;
TAKAI, Y ;
KIMURA, Y ;
SHIMIZU, R ;
IKUTA, T .
ULTRAMICROSCOPY, 1994, 54 (2-4) :261-267
[5]   Size- and support-dependency in the catalysis of gold [J].
Haruta, M .
CATALYSIS TODAY, 1997, 36 (01) :153-166
[6]  
KIMURA Y, 1994, OPTIK, V95, P185
[7]  
TAKASI Y, 1998, CONSTRUCTION APPL EL, P115
[8]  
TANIGUCHI Y, 1992, J ELECTRON MICROSC, V41, P21