Preparation and characteristic of a new class of silica/polyimide nanocomposites

被引:46
作者
Liu, J [1 ]
Gao, Y [1 ]
Wang, FD [1 ]
Li, DC [1 ]
Xu, J [1 ]
机构
[1] Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China
关键词
D O I
10.1023/A:1016002021624
中图分类号
T [工业技术];
学科分类号
08 [工学];
摘要
A new class of silica/polyimide nanocomposites was successfully prepared by the sol-gel reaction, tetraethoxysilane, (TEOS), was hydrolyzed by the water released from imidization at low and high temperature. Silica particles with diameter of around 30-50 nm were observed in the hybrid films by scanning electron microscopy. The flame retardance, decomposition temperature and glass transition temperature of the film increased with increasing silica content. The tensile strength increased slightly while the elongation at break of the films decreased with increasing silica content. (C) 2002 Kluwer Academic Publishers.
引用
收藏
页码:3085 / 3088
页数:4
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