Dichlorobis(1,3-dimethylthiourea-κS)zinc(II)

被引:7
作者
Burrows, AD [1 ]
Harrington, RW [1 ]
Mahon, MF [1 ]
机构
[1] Univ Bath, Dept Chem, Bath BA1 7AY, Avon, England
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2004年 / 60卷
关键词
D O I
10.1107/S1600536804020550
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Determination of the crystal structure of the title compound, [ZnCl2(C3H6N2S)(2)], reveals a distorted tetrahedral geometry around the zinc centre which occupies a twofold axis. Both intra- and intermolecular hydrogen bonding is observed between the 1,3-dimethylthiourea NH groups and the coordinated Cl atoms.
引用
收藏
页码:M1317 / M1318
页数:2
相关论文
共 10 条
[1]   THERMOCHEMISTRY OF THIOUREA COMPLEXES OF TYPE MN(TU)4CL2!, FE(TU)4CL2!, CO(TU)4CL2!, NI(TU)4CL2!, ZN(TU)4CL2!, CD(TU)4CL2!, AND HG(TU)4CL2 [J].
ASHCROFT, SJ .
JOURNAL OF THE CHEMICAL SOCIETY A -INORGANIC PHYSICAL THEORETICAL, 1970, (07) :1020-&
[2]   AN EMPIRICAL CORRECTION FOR ABSORPTION ANISOTROPY [J].
BLESSING, RH .
ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 :33-38
[3]  
*BRUK AXS INC, 2001, SHELXTL VERS 6
[4]   Zinc dicarboxylate polymers and dimers: thiourea substitution as a tool in supramolecular synthesis [J].
Burke, NJ ;
Burrows, AD ;
Donovan, AS ;
Harrington, RW ;
Mahon, MF ;
Price, CE .
DALTON TRANSACTIONS, 2003, (20) :3840-3849
[5]   The influence of hydrogen bonding on the structure of zinc co-ordination polymers [J].
Burrows, AD ;
Harrington, RW ;
Mahon, MF ;
Price, CE .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 2000, (21) :3845-3854
[6]  
BURROWS AD, 2004, IN PRESS EUR J INORG
[7]  
Hooft R. W. W., 1998, COLLECT
[8]   N,N'-DIMETHYLTHIOUREA COMPLEXES OF ZINC, CADMIUM(II), AND MERCURY(II) [J].
MARCOTRIGIANO, G .
ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 1975, 417 (01) :75-80
[9]   Processing of X-ray diffraction data collected in oscillation mode [J].
Otwinowski, Z ;
Minor, W .
MACROMOLECULAR CRYSTALLOGRAPHY, PT A, 1997, 276 :307-326
[10]  
Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR