High yield fabrication of fluorescent nanodiamonds

被引：289

作者：

Boudou, Jean-Paul ^{[1
]}

Curmi, Patrick A. ^{[1
]}

Jelezko, Fedor ^{[2
]}

Wrachtrup, Joerg ^{[2
]}

Aubert, Pascal ^{[3
]}

Sennour, Mohamed ^{[4
]}

Balasubramanian, Gopalakrischnan ^{[2
]}

Reuter, Rolf ^{[2
]}

Thorel, Alain ^{[4
]}

Gaffet, Eric ^{[5
]}

机构：

[1] Univ Evry Val Essonne, INSERM, UEVE U829, F-91025 Evry, France

[2] Univ Stuttgart, Inst Phys 3, D-70550 Stuttgart, Germany

[3] Univ Evry Val Essonne, Nanometr Media Lab, F-91025 Evry, France

[4] ParisTech, Mines Paris, Ctr Mat, F-91000 Evry, France

[5] UTBM, CNRS, UMR 5060, Nanomat Res Grp, F-90010 Belfort, France

来源：

NANOTECHNOLOGY | 2009年 / 20卷 / 23期

关键词：

CHEMICAL-VAPOR-DEPOSITION; DIAMOND THIN-FILMS; NANOCRYSTALLINE DIAMOND; HPHT SYNTHESIS; PARTICLE-SIZE; X-RAY; NITROGEN; VACANCY; NANOPARTICLES; MICROSCOPY;

D O I：

10.1088/0957-4484/20/23/235602

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

A new fabrication method to produce homogeneously fluorescent nanodiamonds with high yields is described. The powder obtained by high energy ball milling of fluorescent high pressure, high temperature diamond microcrystals was converted in a pure concentrated aqueous colloidal dispersion of highly crystalline ultrasmall nanoparticles with a mean size less than or equal to 10 nm. The whole fabrication yield of colloidal quasi-spherical nanodiamonds was several orders of magnitude higher than those previously reported starting from microdiamonds. The results open up avenues for the industrial cost-effective production of fluorescent nanodiamonds with well-controlled properties.

引用

页数：11

共 69 条

[1] Direct interaction of elemental fluorine with diamond surfaces [J].

Ando, T ;

Yamamoto, K ;

Matsuzawa, M ;

Takamatsu, Y ;

Kawasaki, S ;

Okino, F ;

Touhara, H ;

Kamo, M ;

Sato, Y .

[2] Diamond nanoseeding on silicon:: Stability under H2 MPCVD exposures and early stages of growth [J].

Arnault, J. C. ;

Saada, S. ;

Nesladek, M. ;

Williams, O. A. ;

Haenen, K. ;

Bergonzo, P. ;

Osawa, E. .

[3] Nanoscale imaging magnetometry with diamond spins under ambient conditions [J].

Balasubramanian, Gopalakrishnan ;

Chan, I. Y. ;

Kolesov, Roman ;

Al-Hmoud, Mohannad ;

Tisler, Julia ;

Shin, Chang ;

Kim, Changdong ;

Wojcik, Aleksander ;

Hemmer, Philip R. ;

Krueger, Anke ;

Hanke, Tobias ;

Leitenstorfer, Alfred ;

Bratschitsch, Rudolf ;

Jelezko, Fedor ;

Wrachtrup, Joerg .

NATURE, 2008, 455 (7213) :648-U46

[4] Mapping the location and configuration of nitrogen in diamond nanoparticles [J].

Barnard, Amanda S. ;

Sternberg, Michael .

NANOTECHNOLOGY, 2007, 18 (02)

[5] Theory and modeling of nanocarbon phase stability [J].

Barnard, AS .

[6] Substitutional nitrogen in nanodiamond and bucky-diamond particles [J].

Barnard, AS ;

Sternberg, M .

JOURNAL OF PHYSICAL CHEMISTRY B, 2005, 109 (36) :17107-17112

[7] Nonclassical radiation from diamond nanocrystals [J].

Beveratos, A ;

Brouri, R ;

Gacoin, T ;

Poizat, JP ;

Grangier, P .

PHYSICAL REVIEW A, 2001, 64 (06) :4

[8] HPHT synthesis of diamond with high nitrogen content from an Fe3N-C system [J].

Borzdov, Y ;

Pal'yanov, Y ;

Kupriyanov, I ;

Gusev, V ;

Khokhryakov, A ;

Sokol, A ;

Efremov, A .

[9]

BOUDOU JP, 2008, Patent No. 1990313

[10] GROWTH-SECTOR DEPENDENCE OF OPTICAL-FEATURES IN LARGE SYNTHETIC DIAMONDS [J].

BURNS, RC ;

CVETKOVIC, V ;

DODGE, CN ;

EVANS, DJF ;

ROONEY, MLT ;

SPEAR, PM ;

WELBOURN, CM .

JOURNAL OF CRYSTAL GROWTH, 1990, 104 (02) :257-279

← 1 2 3 4 5 6 7 →