129Xe NMR spectrum of xenon inside C60

被引:131
作者
Syamala, MS [1 ]
Cross, RJ [1 ]
Saunders, M [1 ]
机构
[1] Yale Univ, Dept Chem, New Haven, CT 06520 USA
关键词
D O I
10.1021/ja012676f
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Xenon was inserted into C-60 by heating C-60 in 3000 atm of xenon gas at 650 degreesC. The Xe @ C-60 was separated from the empty C-60 by using HPLC. The C-13 resonance for Xe @ C-60 is shifted downfield by 0.95 ppm (192 Hz). Xe-129 NMR showed a line 179.2 ppm downfield from xenon gas.
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页码:6216 / 6219
页数:4
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