Zirconia-toughened hydroxyapatite ceramic obtained by wet sintering

被引:43
作者
Delgado, JA
Morejón, L
Martínez, S [1 ]
Ginebra, MP
Carlsson, N
Fernández, E
Planell, JA
Clavaguera-Mora, MT
Rodríguez-Viejo, J
机构
[1] Univ Barcelona, Fac Geol, Dept Cristallog Mineral, E-08028 Barcelona, Spain
[2] Univ Barcelona, Fac Geol, Dipartimento Minerals, E-08028 Barcelona, Spain
[3] Univ Politecn Catalunya, Dept Mat Sci & Met Engn, CREB, E-08028 Barcelona, Spain
[4] Univ Autonoma Barcelona, Dept Fis, Grp Fis Mat 1, E-08193 Barcelona, Spain
[5] Univ Habana, Ctr Biomat, Ciudad Habana 10400, Cuba
关键词
D O I
10.1023/A:1008923121172
中图分类号
R318 [生物医学工程];
学科分类号
0831 ;
摘要
A toughened hydroxyapatite (HA) ceramic has been obtained through the incorporation of magnesia partially stabilized zirconia (Mg-PSZ) under uniaxial pressing and sintering in wet oxygen at 1250 degrees C for 4 h. The powder X-ray diffraction (XRD) patterns and infrared spectra (FT-IR) show that HA is the only calcium phosphate phase present. The composite (MgPSZ-HA) has a density of 94% the theoretical value. The bending strength and the fracture toughness are around 50% higher for Mg-PSZ reinforced than for HA. The grain size and the fracture surface were studied by scanning electron microscopy (SEM). The influence of the Mg-PSZ particles on the fracture mechanism of the HA ceramic is discussed. (C) 1999 Kluwer Academic Publishers.
引用
收藏
页码:715 / 719
页数:5
相关论文
共 18 条
[1]   Monoclinic phase measurement in Mg-PSZ using X-ray diffraction [J].
Batchelor, WJ ;
Finlayson, TR ;
Kelly, GL .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1996, 79 (09) :2477-2480
[2]   MICROSTRUCTURAL DESIGN OF TOUGHENED CERAMICS [J].
BECHER, PF .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1991, 74 (02) :255-269
[3]  
CAETANOZURITA J, 1994, P 7 INT S CER MED JU, P267
[4]  
De Groot K., 1981, SCI CERAM, V11, P433
[5]   PERSPECTIVE ON THE DEVELOPMENT OF HIGH-TOUGHNESS CERAMICS [J].
EVANS, AG .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1990, 73 (02) :187-206
[6]  
GARCIAMENOCAL JAD, 1999, P TOP S 11 MAT CLIN, P259
[7]   The measurement of surface contact fatigue and its application to engineering ceramics [J].
Guillou, MO ;
Henshall, JL ;
Hooper, RM .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1996, 209 (1-2) :116-127
[8]   MICROSTRUCTURE AND MECHANICAL-PROPERTIES OF HYDROXYAPATITE CERAMICS WITH ZIRCONIA DISPERSION PREPARED BY POST-SINTERING [J].
IOKU, K ;
YOSHIMURA, M ;
SOMIYA, S .
BIOMATERIALS, 1990, 11 (01) :57-61
[9]  
KASUGA T, 1993, J MATER SCI-MATER M, V4, P3
[10]   PREPARATION AND THERMAL-PROPERTIES OF DENSE POLYCRYSTALLINE OXYHYDROXYAPATITE [J].
KIJIMA, T ;
TSUTSUMI, M .
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1979, 62 (9-10) :455-460