Use of multiple-edge refinement of extended x-ray absorption fine structure to determine site occupancy in mixed ferrite nanoparticles

被引:44
作者
Calvin, S [1 ]
Carpenter, EE
Harris, VG
Morrison, SA
机构
[1] USN, Res Lab, Washington, DC 20375 USA
[2] George Washington Univ, Washington, DC 20052 USA
关键词
D O I
10.1063/1.1520700
中图分类号
O59 [应用物理学];
学科分类号
摘要
The site occupancy of manganese zinc ferrite (MZFO) nanoparticles is determined by a multiple-edge refinement of the extended x-ray absorption fine structure of the manganese, zinc, and iron absorption edges. The MZFO nanoparticles are generated by a reverse micellar synthetic route and compared to a ceramic standard. The simultaneous fitting of multiple absorption edges to a constrained model is found to yield site occupancies accurate to within eight percentage points. (C) 2002 American Institute of Physics.
引用
收藏
页码:3828 / 3830
页数:3
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