Separation and determination of volatile compounds in synthetic wine samples by gas chromatography using UV-visible molecular absorption spectrometry as detector

被引:16
作者
Cedrón-Fernández, T
Sáenz-Barrio, C
Cabredo-Pinillos, S
Sanz-Vicente, I
机构
[1] Univ La Rioja, Dept Quim Quim Analit, Edificio Cient Tecnol, Logrono 26006, Spain
[2] Univ Zaragoza, Fac Ciencias, Dept Quim Analit, E-50009 Zaragoza, Spain
关键词
gas chromatography; EAM-UV-Vis detector; wine samples; volatile compounds;
D O I
10.1016/S0039-9140(02)00055-3
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
This paper shows the separation and determination of eight compounds containing the OH group (ethanol, pentanol, 3-methyl-1-butanol, hexanol, phenol, benzyl-alcohol, phenylethanol and geraniol) in synthetic wine by gas chromatography using UV-Vis molecular absorption spectrometry as detection system. All the parameters affecting the separation and determination were optimised using some methods of experiment design. The analytical characteristics of each compound were calculated and detection limits ranging from 2.3 to 74 mg l(-1) have been obtained. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:555 / 563
页数:9
相关论文
共 27 条
[1]  
[Anonymous], [No title captured]
[2]   ANALYSIS OF WINE AROMA BY OFF-LINE AND ONLINE SUPERCRITICAL-FLUID EXTRACTION GAS-CHROMATOGRAPHY [J].
BLANCH, GP ;
REGLERO, G ;
HERRAIZ, M .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1995, 43 (05) :1251-1257
[3]   REMOTE SCANNING ULTRAVIOLET DETECTION FOR CAPILLARY GAS-CHROMATOGRAPHY [J].
BORNHOP, DJ ;
HLOUSEK, L ;
HACKETT, M ;
WANG, H ;
MILLER, GC .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1992, 63 (01) :191-201
[4]  
BORNHOP DJ, 1994, J CHROMATOGR A, V684, P259
[5]   RAPID EXTRACTION OF AROMA COMPOUNDS IN MUST AND WINE BY MEANS OF ULTRASOUND [J].
COCITO, C ;
GAETANO, G ;
DELFINI, C .
FOOD CHEMISTRY, 1995, 52 (03) :311-320
[6]  
De La Calle Garcia D., 1999, APPL SOLID PHASE MIC, P372
[7]  
DIAZREGANON MD, 1995, SCI ALIMENT, V15, P187
[8]   CAPILLARY GAS-CHROMATOGRAPHIC ANALYSIS WITH THE FAR-UV ABSORBANCE DETECTOR [J].
DRISCOLL, JN ;
DUFFY, M ;
PAPPAS, S .
JOURNAL OF CHROMATOGRAPHY, 1988, 441 (01) :63-71
[9]  
ETIEVANT PX, 1991, VOLATILE COMPOUNDS F, pCH14
[10]  
García DD, 1998, VITIS, V37, P181