Towards the rehabilitation of the Leuckart reductive amination reaction using microwave technology.

被引：55

作者：

Loupy, A ^{[1
]}

Monteux, D ^{[1
]}

Petit, A ^{[1
]}

Aizpurua, JM ^{[1
]}

Dominguez, E ^{[1
]}

Palomo, C ^{[1
]}

机构：

[1] UNIV BASQUE COUNTRY, FAC QUIM, DEPT QUIM ORGAN, SAN SEBASTIAN 20080, SPAIN

来源：

TETRAHEDRON LETTERS | 1996年 / 37卷 / 45期

关键词：

D O I：

10.1016/0040-4039(96)01865-5

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Leuckart reductive amination of carbonyl compounds was dramatically enhanced with respect to conventional heating by a specific microwave effect when the reaction was performed, under solvent-free conditions, in a monomode microwave reactor. Excellent isolated yields (up to 97%) were attained within short reaction times (typically, 30 minutes) Copyright (C) 1996 Published by Elsevier Science Ltd

引用

页码：8177 / 8180

页数：4

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