Synthesis and characterisation of iodo functionalised ytterbium(II) and ytterbium(III) alkoxides

被引:34
作者
Duncalf, DJ [1 ]
Hitchcock, PB [1 ]
Lawless, GA [1 ]
机构
[1] UNIV SUSSEX,SCH CHEM & MOLEC SCI,BRIGHTON BN1 9QJ,E SUSSEX,ENGLAND
关键词
D O I
10.1039/cc9960000269
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The reaction of YbI2 in thf with an equimolar quantity of K(OCPh(3)) affords [{YbI(mu-OCPh(3))(eta(2)-dme)}(2)] 1; upon photolysis, YbI2 reacts with dme and yields [{YbI2(mu OMe)(eta(2)-dme}(2)] 2; the solid-state structures of 1 and 2 are determined.
引用
收藏
页码:269 / 271
页数:3
相关论文
共 33 条
[1]   THE 1ST HIGH-RESOLUTION DIRECT NMR OBSERVATION OF AN F-BLOCK ELEMENT [J].
AVENT, AG ;
EDELMAN, MA ;
LAPPERT, MF ;
LAWLESS, GA .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1989, 111 (09) :3423-3425
[2]   SYNTHESIS AND STRUCTURE OF ORGANOSILICON AND ORGANOGERMANIUM COMPLEXES OF YTTERBIUM (PH3E)2YB(THF)4 WITH YB-SI AND YB-GE BONDS [J].
BOCHKAREV, LN ;
MAKAROV, VM ;
HRZHANOVSKAYA, YN ;
ZAKHAROV, LN ;
FUKIN, GK ;
YANOVSKY, AI ;
STRUCHKOV, YT .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1994, 467 (02) :C3-C5
[3]   SYNTHESIS AND STRUCTURE OF A COMPOUND WITH AN YTTERBIUM TIN BOND, (PH3SN)2YB(THF)4 [J].
BOCHKAREV, MN ;
KHRAMENKOV, VV ;
RADKOV, YF ;
ZAKHAROV, LN ;
STRUCHKOV, YT .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1991, 408 (03) :329-334
[4]   SYNTHESIS AND STRUCTURE OF BIS(TRIPHENYLGERMANE)TETRAKIS-(TETRAHYDROFURAN)YTTERBIUM [J].
BOCHKAREV, MN ;
PENYAGINA, IM ;
ZAKHAROV, LN ;
RADKOV, YF ;
FEDOROVA, EA ;
KHORSHEV, SY ;
STRUCHKOV, YT .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1989, 378 (03) :363-373
[5]   PENTANUCLEAR OXOALKOXIDE CLUSTERS OF SCANDIUM, YTTRIUM, INDIUM AND YTTERBIUM, X-RAY CRYSTAL-STRUCTURES OF [M5(MU5-O)(MU3-OPRI)4 (MU2-OPRI)4(OPRI)5] (M = IN, YB) [J].
BRADLEY, DC ;
CHUDZYNSKA, H ;
FRIGO, DM ;
HAMMOND, ME ;
HURSTHOUSE, MB ;
MAZID, MA .
POLYHEDRON, 1990, 9 (05) :719-726
[6]   PYRIDINE COORDINATION-COMPLEXES OF THE DIVALENT YTTERBIUM CHALCOGENOLATES YB(EPH)2 (E=S, SE, TE) [J].
BREWER, M ;
KHASNIS, D ;
BURETEA, M ;
BERARDINI, M ;
EMGE, TJ ;
BRENNAN, JG .
INORGANIC CHEMISTRY, 1994, 33 (13) :2743-2747
[7]  
CETINKAYA B, 1992, J CHEM SOC CHEM COMM, P932
[8]   THE 1ST STRUCTURALLY AUTHENTICATED DIVALENT LANTHANIDE STANNYL DERIVATIVE [J].
CLOKE, FGN ;
DALBY, CI ;
HITCHCOCK, PB ;
KARAMALLAKIS, H ;
LAWLESS, GA .
JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1991, (11) :779-781
[9]   ORGANOAMIDO-LANTHANOIDS AND ARYLOXO-LANTHANOIDS .5. PREPARATIONS OF LOW-COORDINATE LANTHANOID(II) PHENOLATES, LN(OC6H2BU(T)2-2,6-X-4)2(THF)N (LN = YB OR EU - X = H, ME OR BU(T) - N = 2 OR 3) AND THE X-RAY CRYSTAL-STRUCTURE OF 5-COORDINATE [YB(OC6H2BU(T)3-2,4,6)2(THF)3].THF [J].
DEACON, GB ;
FENG, T ;
MACKINNON, P ;
NEWNHAM, RH ;
NICKEL, S ;
SKELTON, BW ;
WHITE, AH .
AUSTRALIAN JOURNAL OF CHEMISTRY, 1993, 46 (03) :387-399
[10]   ORGANOLANTHANOIDS .5. THE CRYSTAL AND MOLECULAR-STRUCTURE OF DI-ETA-5-CYCLOPENTADIENYL-1,2-DIMETHOXYETHANEYTTERBIUM(II) [J].
DEACON, GB ;
MACKINNON, PI ;
HAMBLEY, TW ;
TAYLOR, JC .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1983, 259 (01) :91-97