Determining temperature in a magic-angle spinning probe using the temperature dependence of the isotropic chemical shift of lead nitrate

被引:88
作者
Neue, G
Dybowski, C
机构
[1] UNIV DORTMUND,DORTMUND,GERMANY
[2] UNIV DELAWARE,DEPT CHEM & BIOCHEM,NEWARK,DE 19716
关键词
temperature; calibration; lead nitrate; magic-angle spinning;
D O I
10.1016/S0926-2040(96)01291-X
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The calibration of temperature in a magic-angle spinning probe with lead nitrate is discussed. The effects of rotation frequency on temperature are demonstrated. (C) 1997 Elsevier Science B.V.
引用
收藏
页码:333 / 336
页数:4
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