Grazing-incidence small-angle X-ray scattering applied to the characterization of aggregates in surface regions

被引:57
作者
Naudon, A
Babonneau, D
Thiaudière, D
Lequien, S
机构
[1] Univ Poitiers, Met Phys Lab, UMR 6630 CNRS, UFR Sci, F-86962 Futuroscope Chasseneuil, France
[2] European Synchrotron Radiat Facil, F-38043 Grenoble, France
[3] CEA Saclay, CEA CNRS, Lab Pierre Sue, F-91191 Gif Sur Yvette, France
来源
PHYSICA B | 2000年 / 283卷 / 1-3期
关键词
grazing incidence; X-ray scattering; thin film growth; ion assistance;
D O I
10.1016/S0921-4526(99)01894-3
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
Ion-beam sputtering deposition has been used to elaborate discontinuous gold and granular carbon-platinum thin films. The morphology of the deposited gold islands and buried platinum clusters so obtained has been studied by grazing incidence small-angle X-ray scattering (GISAXS). The full potentiality of this non-destructive technique at grazing incidence is obtained when it is coupled with a synchrotron radiation beam and two-dimensional detectors. The influence of argon ion-implantation performed during Au or C-Pt growth has been studied. A relevant information to understand and control the structural properties of such materials is then achieved. (C) 2000 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:69 / 74
页数:6
相关论文
共 19 条
[1]   TEM AND AFM STUDY OF GOLD THIN-FILM NUCLEATION AND GROWTH [J].
ARNAULT, JC ;
TEMPLIER, C ;
DELAFOND, J ;
BOUFFARD, S ;
GAREM, H .
SURFACE & COATINGS TECHNOLOGY, 1995, 71 (01) :45-52
[2]   Microstructural study of a C-Fe alloy synthesized by ion-beam sputtering co-deposition [J].
Babonneau, D ;
Cabioc'h, T ;
Denanot, MF ;
Naudon, A .
APPLIED PHYSICS LETTERS, 1999, 74 (06) :800-802
[3]   Silver nanoparticles encapsulated in carbon cages obtained by co-sputtering of the metal and graphite [J].
Babonneau, D ;
Cabioc'h, T ;
Naudon, A ;
Girard, JC ;
Denanot, MF .
SURFACE SCIENCE, 1998, 409 (02) :358-371
[4]   Co-sputtering C-Cu thin film synthesis:: microstructural study of copper precipitates encapsulated into a carbon matrix [J].
Cabioc'h, T ;
Naudon, A ;
Jaouen, M ;
Thiaudiére, D ;
Babonneau, D .
PHILOSOPHICAL MAGAZINE B-PHYSICS OF CONDENSED MATTER STATISTICAL MECHANICS ELECTRONIC OPTICAL AND MAGNETIC PROPERTIES, 1999, 79 (03) :501-516
[5]   ASAX SPECTROMETER [J].
DUBUISSON, JM ;
DAUVERGNE, JM ;
DEPAUTEX, C ;
VACHETTE, P ;
WILLIAMS, CE .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1986, 246 (1-3) :636-640
[6]   SURFACE-STRUCTURE DETERMINATION BY X-RAY-DIFFRACTION [J].
FEIDENHANSL, R .
SURFACE SCIENCE REPORTS, 1989, 10 (03) :105-188
[7]   CALIBRATION AND CORRECTION OF SPATIAL DISTORTIONS IN 2D DETECTOR SYSTEMS [J].
HAMMERSLEY, AP ;
SVENSSON, SO ;
THOMPSON, A .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1994, 346 (1-2) :312-321
[8]   2 ORIGINAL PIECES OF APPARATUS FOR THE PREPARATION OF COATINGS USING DYNAMIC ION-BEAM MIXING - 1ST APPLICATIONS [J].
JAULIN, M ;
LAPLANCHE, G ;
DELAFOND, J ;
PIMBERTMICHAUX, S .
SURFACE & COATINGS TECHNOLOGY, 1989, 37 (02) :225-235
[9]   Small-angle X-ray scattering experiments in grazing incidence on sol-gel coatings containing nano-scaled colloids: A new technique for investigating thin coatings and films [J].
Kutsch, B ;
Lyon, O ;
Schmitt, M ;
Mennig, M ;
Schmidt, H .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1997, 30 :948-956
[10]   DESIGN OF THE ANOMALOUS SCATTERING BEAMLINE AT THE EUROPEAN SYNCHROTRON-RADIATION FACILITY [J].
LEQUIEN, S ;
GOIRAND, L ;
LESIMPLE, F .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1995, 66 (02) :1725-1727