Facile synthesis of stable magnetic fluid using size-controlled Fe3O4 nanoparticles

被引:13
作者
Bateer, Buhe [1 ,2 ]
Qu, Yang [1 ]
Tian, Chungui [1 ]
Du, Shichao [1 ]
Ren, Zhiyu [1 ]
Wang, Ruihong [1 ]
Pan, Kai [1 ]
Fu, Honggang [1 ]
机构
[1] Heilongjiang Univ, Minist Educ Peoples Republ China, Key Lab Funct Inorgan Mat Chem, Harbin 150080, Peoples R China
[2] Heilongjiang Inst Technol, Sch Mat & Chem Engn, Harbin 150050, Peoples R China
基金
中国国家自然科学基金; 高等学校博士学科点专项科研基金;
关键词
Magnetic materials; Nanostructures; Magnetic properties; Surface properties; MFE2O4; M; FE; CO;
D O I
10.1016/j.materresbull.2014.04.044
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Magnetic fluids based on superparamagnetic, well-crystalline and mono-dispersed Fe3O4 nanoparticles are synthesized by a facile thermal decomposition method. Low-cost Fe(oleate)(3) is used as ferrous resource, and paraffin oil is introduced as solvent and carrier simultaneously. Fe3O4 nanoparticles with three kinds of different size (12, 16 and 20 nm), exhibiting different saturation magnetization of 65.51, 68.03 and 74.48 emu/g, respectively, are prepared easily by controlling the thermal decomposition time. Magnetic performance and viscosity-temperature characteristics of the magnetic fluid are also studied. It is found that the saturation magnetization of the magnetic fluid with 5% Fe3O4 mass percentage is 2.94 emu/g, which exhibits a good viscosity temperature characteristics compared with paraffin carrier. (C) 2014 Elsevier Ltd. All rights reserved.
引用
收藏
页码:34 / 38
页数:5
相关论文
共 28 条
[1]   A facile thermolysis route to monodisperse ferrite nanocrystals [J].
Bao, Ningzhong ;
Shen, Liming ;
Wang, Yuhsiang ;
Padhan, Prahallad ;
Gupta, Arunava .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2007, 129 (41) :12374-+
[2]   Preparation and magnetic performance of the magnetic fluid stabilized by bi-surfactant [J].
Bateer, Buhe ;
Qu, Yang ;
Meng, Xiangying ;
Tian, Chungui ;
Du, Shichao ;
Wang, Ruihong ;
Pan, Kai ;
Fu, Honggang .
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2013, 332 :151-156
[3]  
Borduz L., 2001, U.S. Patent, Patent No. [6,277,298B1, 6277298]
[4]  
Buschow K H.J., 2006, Handbook of Magnetic Materials
[5]   Effects of shear rate and particle concentration on rheological properties of magnetic particle suspensions [J].
Choi, HJ ;
Kwon, TM ;
Jhon, MS .
JOURNAL OF MATERIALS SCIENCE, 2000, 35 (04) :889-894
[6]  
Cullity B. D., 1978, ELEMENTS XRAY DIFFRA
[7]   Hydrothermal synthesis of monodisperse magnetite nanoparticles [J].
Daou, T. J. ;
Pourroy, G. ;
Begin-Colin, S. ;
Greneche, J. M. ;
Ulhaq-Bouillet, C. ;
Legare, P. ;
Bernhardt, P. ;
Leuvrey, C. ;
Rogez, G. .
CHEMISTRY OF MATERIALS, 2006, 18 (18) :4399-4404
[8]   Synthesis and application of hollow magnetic graphitic carbon microspheres with/without TiO2 nanoparticle layer on the surface [J].
Feng, Shanshan ;
Ren, Zhiyu ;
Wei, Yuanlong ;
Jiang, Baojiang ;
Liu, Yang ;
Zhang, Lingyi ;
Zhang, Weibing ;
Fu, Honggang .
CHEMICAL COMMUNICATIONS, 2010, 46 (34) :6276-6278
[9]   ZnFe2O4 nanoparticles for ferrofluids: A combined XANES and XRD study [J].
Gomes, J. A. ;
Azevedo, G. M. ;
Depeyrot, J. ;
Mestnik-Filho, J. ;
da Silva, G. J. ;
Tourinho, F. A. ;
Perzynski, R. .
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2011, 323 (10) :1203-1206
[10]   Controlled Synthesis of Iron Oxide Nanoparticles over a Wide Size Range [J].
Guardia, Pablo ;
Perez, Nicolas ;
Labarta, Amilcar ;
Batlle, Xavier .
LANGMUIR, 2010, 26 (08) :5843-5847