SO3H-functionalized silica for acetalization of carbonyl compounds with methanol and tetrahydropyranylation of alcohols

被引：100

作者：

Shimizu, K

Hayashi, E

Hatamachi, T

Kodama, T

Kitayama, Y

机构：

[1] Niigata Univ, Fac Engn, Dept Chem & Chem Engn, Niigata 9502181, Japan

[2] Niigata Univ, Grad Sch Sci & Technol, Niigata 9502181, Japan

来源：

TETRAHEDRON LETTERS | 2004年 / 45卷 / 26期

关键词：

acetalization; tetrahydropyranylation; catalysis; meso-porous silica; sulfonic acid;

D O I：

10.1016/j.tetlet.2004.04.186

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Sulfonic acid group-functionalized amorphous silica acts as a highly effective and reusable catalyst for acetalization of various carbonyl compounds with methanol and tetrahydropyranylation of alcohols. (C) 2004 Elsevier Ltd. All rights reserved.

引用

页码：5135 / 5138

页数：4

共 35 条

[1]

ALPER H, 1972, SYNTH-INT J METHODS, P81

[2] SILICA-BOUND SULFONIC-ACID CATALYSTS [J].

BADLEY, RD ;

FORD, WT .

JOURNAL OF ORGANIC CHEMISTRY, 1989, 54 (23) :5437-5443

[3] 1,3-dioxolanes from carbonyl compounds over zeolite HSZ-360 as a reusable, heterogeneous catalyst [J].

Ballini, R ;

Bosica, G ;

Frullanti, B ;

Maggi, R ;

Sartori, G ;

Schroer, F .

TETRAHEDRON LETTERS, 1998, 39 (12) :1615-1618

[4] Solvent free tetrahydropyranylation of phenols and alcohols over zeolites HSZ as reusable catalysts [J].

Ballini, R ;

Bigi, F ;

Carloni, S ;

Maggi, R ;

Sartori, G .

TETRAHEDRON LETTERS, 1997, 38 (23) :4169-4172

[5]

BONGINI A, 1979, SYNTHESIS-STUTTGART, P618

[6] SPANISH SEPIOLITE CLAY AS A NEW HETEROGENEOUS CATALYST FOR THE TETRAHYDROPYRANYLATION OF ALCOHOLS AND PHENOLS [J].

CAMPELO, JM ;

GARCIA, A ;

LAFONT, F ;

LUNA, D ;

MARINAS, JM .

SYNTHETIC COMMUNICATIONS, 1994, 24 (10) :1345-1350

[7] SMALL-RING COMPOUNDS .21. 3-METHYLENECYCLOBUTANONE AND RELATED COMPOUNDS [J].

CASERIO, FF ;

ROBERTS, JD .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1958, 80 (21) :5837-5840

[8] Zeolites for the production of fine chemicals: Synthesis of the fructone fragrancy [J].

Climent, MJ ;

Corma, A ;

Velty, A ;

Susarte, M .

JOURNAL OF CATALYSIS, 2000, 196 (02) :345-351

[9] FORMATION AND HYDROLYSIS OF ACETALS CATALYZED BY ACID FAUJASITES [J].

CORMA, A ;

CLIMENT, MJ ;

CARCIA, H ;

PRIMO, J .

APPLIED CATALYSIS, 1990, 59 (02) :333-340

[10] Sulfonic acid functionalized mesoporous MCM-41 silica as a convenient catalyst for Bisphenol-A synthesis [J].

Das, D ;

Lee, JF ;

Cheng, SF .

CHEMICAL COMMUNICATIONS, 2001, (21) :2178-2179

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