Synthesis, structure and reactivity of [Yb(eta-C(5)Me(5)){Si(SiMe(3))(3)}(thf)(2)]

被引：40

作者：

Corradi, MM ^{[1
]}

Frankland, AD ^{[1
]}

Hitchcock, P ^{[1
]}

Lappert, MF ^{[1
]}

Lawless, GA ^{[1
]}

机构：

[1] UNIV SUSSEX,CHEM LAB,SCH CHEM PHYS & ENVIRONM SCI,BRIGHTON BN1 9QJ,E SUSSEX,ENGLAND

来源：

CHEMICAL COMMUNICATIONS | 1996年 / 20期

关键词：

D O I：

10.1039/cc9960002323

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The reaction of [Yb(eta C(5)Me(5))(2)(OEt(2))] With 1 equiv, of [Li{Si(SiMe(3))(3)} (thf)(3)] in toluene affords [Yb(eta-C(5)Me(5)){Si-(SiMe(3))(3)}(thf)(2)] 1 in high yield; a single-crystal X-ray analysis and multinuclear Yb-171 and Si-29 NMR spectroscopic data for 1 are reported.

引用

页码：2323 / 2324

页数：2

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