Rapid preparation of YBa2Cu3O7-x with T-c similar to 90 K using a domestic microwave oven

被引:22
作者
Kato, M
Sakakibara, K
Koike, Y
机构
来源
JAPANESE JOURNAL OF APPLIED PHYSICS PART 2-LETTERS & EXPRESS LETTERS | 1997年 / 36卷 / 10A期
关键词
domestic microwave oven; YBa2Cu3O7-x; sample preparation; high-T-c superconductor; electrical resistivity; magnetic susceptibility;
D O I
10.1143/JJAP.36.L1291
中图分类号
O59 [应用物理学];
学科分类号
摘要
High-T-c superconducting samples of YBa2Cu3O7-x with T-c similar to 90 K have been prepared in a short time of 25 min, using a domestic microwave oven operated at 2.45 GHz and 200 W, without any post-heat treatment. Post-heat treatment is not necessary due to improvement of the sample environment during the microwave process. That is, a pellet of mixed powders of raw materials is surrounded by mixed powders of raw materials and subsequently wrapped in glass wool, in order to suppress rapid dissipation of heat from the surface of the pellet. This leads to successful preparation of homogeneous and oxygenated samples of YBa2Cu3O7-x.
引用
收藏
页码:L1291 / L1293
页数:3
相关论文
共 9 条
  • [1] ANISIMOVA NY, 1996, RUSS J INORG CHEM, V41, P179
  • [2] MICROWAVE SYNTHESES FOR SUPERCONDUCTING CERAMICS
    BAGHURST, DR
    CHIPPINDALE, AM
    MINGOS, DMP
    [J]. NATURE, 1988, 332 (6162) : 311 - 311
  • [3] APPLICATION OF MICROWAVE-HEATING TECHNIQUES FOR THE SYNTHESIS OF SOLID-STATE INORGANIC-COMPOUNDS
    BAGHURST, DR
    MINGOS, DMP
    [J]. JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1988, (12) : 829 - 830
  • [4] SELF-PROPAGATING HIGH-TEMPERATURE SYNTHESIS (SHS) AND MICROWAVE-ASSISTED COMBUSTION SYNTHESIS (MACS) OF THE THALLIUM SUPERCONDUCTING PHASES
    BAYYA, SS
    SNYDER, RL
    [J]. PHYSICA C, 1994, 225 (1-2): : 83 - 90
  • [5] MICROWAVE SYNTHESIS OF HIGH-TC SUPERCONDUCTORS
    FELDSTEIN, H
    BENDOR, L
    BEILIN, V
    [J]. PHYSICA C, 1994, 235 : 929 - 930
  • [6] HIGH-TC SUPERCONDUCTOR YBA2CU3OY - OXYGEN-CONTENT VS TC RELATION
    TAKAYAMAMUROMACHI, E
    UCHIDA, Y
    ISHII, M
    TANAKA, T
    KATO, K
    [J]. JAPANESE JOURNAL OF APPLIED PHYSICS PART 2-LETTERS & EXPRESS LETTERS, 1987, 26 (07): : L1156 - L1158
  • [7] FAST SOLID-STATE SYNTHESIS OF METAL VANADATES AND CHALCOGENIDES USING MICROWAVE IRRADIATION
    VAIDHYANATHAN, B
    GANGULI, M
    RAO, KJ
    [J]. MATERIALS RESEARCH BULLETIN, 1995, 30 (09) : 1173 - 1177
  • [8] MICROSTRUCTURE DEVELOPMENT IN REPEATED ZONE-REFINING OF MICROWAVE-DERIVED YBCO BULK COMPACTS
    VARMA, HK
    WARRIER, KG
    KUMAR, VA
    MANI, TV
    PILLAI, SPGK
    DAMODARAN, AD
    [J]. JAPANESE JOURNAL OF APPLIED PHYSICS PART 2-LETTERS, 1992, 31 (5A): : L543 - L546
  • [9] RAPID METHOD FOR THE PREPARATION OF 123 SUPERCONDUCTOR USING MICROWAVES
    WARRIER, KGK
    VARMA, HK
    MANI, TV
    DAMODARAN, AD
    [J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1992, 75 (07) : 1990 - 1992