Effect of sintering temperature on the characteristics of carbons based on mesocarbon microbeads

被引:26
作者
Bhatia, G
Aggarwal, RK
Punjabi, N
Bahl, OP
机构
[1] Carbon Technology Unit, National Physical Laboratory, New Delhi 110012, Dr K. S. Krishnan Road
关键词
Polymer; Porosity; Heat Treatment; Shrinkage; Solvent Extraction;
D O I
10.1023/A:1018587418496
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A study was conducted to determine the effect of sintering temperature, ranging between 350 and 2700 degrees C, on the characteristics of carbons made from mesocarbon microbeads (MCMB) of size 4-16 mu m, formed in a coal tar pitch by heat treatment at 420 degrees C for 2.5 h, and separated by solvent extraction using a tar oil. It was found that the MCMB-based carbon plates heat treated to 1000 and 2700 degrees C possess, respectively, an apparent density of 1.64 and 1.78 g cm(-3), a weight loss of 11.5% and 15.3%, a volume shrinkage of 32.4% and 45.0%, an open porosity of 7.6% and 14.0%, a bending strength of 72 and 50 MPa, and an atomic C/H ratio of 30 and 417. The 2700 degrees C heat-treated plates revealed homogeneity and fine isotropic structure.
引用
收藏
页码:135 / 139
页数:5
相关论文
共 14 条
[1]   FORMATION OF MESOPHASE SPHERULES IN LOW-QL COAL-TAR PITCHES AND DEVELOPMENT OF MONOLITHIC CARBONS THEREFROM [J].
BHATIA, G ;
AGGARWAL, RK ;
PUNJABI, N ;
BAHL, OP .
JOURNAL OF MATERIALS SCIENCE, 1994, 29 (18) :4757-4763
[2]  
BHATIA G, 1992, P NAT WORKSH NEW CAR, P398
[3]  
BHATIA G, 1994, P NAT C CARB 94, P186
[4]  
BHATIA G, 1993, 21 BIENN CARB C AM C, P719
[5]  
BHATIA G, 1991, 2 ANN GEN M MAT RES
[6]  
BHATIA G, 1989, P IND WORKSH PITCH P, P22
[7]  
FUKUDA N, 1988, P INT C CARB, P620
[8]  
HONDA H, 1973, CERAMIC DATA BOOK, P377
[9]  
Honda H., 1973, J JPN PETROL INST, V16, P392
[10]  
MORRIS C, 1989, P 19 BIENN C CARB AM, P142