New synthesis of phenyl-substituted 2,3-dihydro-1,3-dithiolo[4,5-e][1,4]dithiin-6-thione

被引：18

作者：

Noh, DY

Lee, HJ

Hong, JK

Underhill, AE

机构：

[1] KOREA BASIC SCI INST,MASS SPECTOMETRY GRP,TAEJON 305600,SOUTH KOREA

[2] UNIV COLL N WALES,DEPT CHEM,BANGOR LL57 2UW,GWYNEDD,WALES

来源：

TETRAHEDRON LETTERS | 1996年 / 37卷 / 42期

基金：

英国工程与自然科学研究理事会;

关键词：

D O I：

10.1016/0040-4039(96)01672-3

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The facile synthesis of 4 and (+/-)-6 was carried oat via a Diels-Alder type [2+4] cycloaddition reaction of oligomeric dien 8 with styrene or t-stilbene, respectively, as a dienophile by a thermal reaction and/or photoreaction. (+/-)-6 crystallized as a racemic compound composed of (2R,3R) and (2S,3S) enantiomers. Copyright (C) 1996 Elsevier Science Ltd

引用

页码：7603 / 7606

页数：4

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[3]

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[4] NEW PI-DONOR PRECURSOR MOLECULE FOR THE PREPARATION OF ORGANIC METALS, 4,5-4',5'-BIS(1,4-DIOXANEDIYL-2,3-DITHIO)-TETRATHIAFULVALENE - SYNTHESIS AND PROPERTIES [J].