Gradient flow titration for the determination of fluoride ion in natural waters

被引:9
作者
da Conceiçao, AC
dos Santos, MMC
Gonçalves, MLSS
Santos, FJV
机构
[1] Inst Super Tecn, Ctr Quim Estrutural, P-1049001 Lisbon, Portugal
[2] Univ Lisbon, Fac Ciencias, Dept Quim & Bioquim, P-1700 Lisbon, Portugal
关键词
gradient flow titration; fluoride; water analysis;
D O I
10.1016/S0039-9140(99)00236-2
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The determination of fluoride ions in water samples was accomplished by using a gradient flow titration. A standard commercial combined electrode is used in a cell configuration that combines the gradient chamber and the electrode in a single unit. The methodology developed gives results with a relative standard deviation of about 3%. The average recoveries after spiking natural samples with fluoride are in the range 100-102%. The method was used successful in determining the fluoride concentration in water samples. (C) 2000 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:1245 / 1252
页数:8
相关论文
共 14 条
[1]  
[Anonymous], 1995, Standard methods for the examination of water and wastewater, V19th
[2]   FLUORIDE ION-SELECTIVE ELECTRODE IN FLOW-INJECTION ANALYSIS .2. INTERFERENCE STUDIES [J].
FRENZEL, W ;
BRATTER, P .
ANALYTICA CHIMICA ACTA, 1986, 187 :1-16
[3]   THE FLUORIDE ION-SELECTIVE ELECTRODE IN FLOW-INJECTION ANALYSIS .3. APPLICATIONS [J].
FRENZEL, W ;
BRATTER, P .
ANALYTICA CHIMICA ACTA, 1986, 188 :151-164
[4]   THE FLUORIDE ION-SELECTIVE ELECTRODE IN FLOW-INJECTION ANALYSIS .1. GENERAL METHODOLOGY [J].
FRENZEL, W ;
BRATTER, P .
ANALYTICA CHIMICA ACTA, 1986, 185 :127-136
[5]   APPLICATION OF ION-SELECTIVE ELECTRODES IN ENVIRONMENTAL-ANALYSIS DETERMINATION OF ACID AND FLUORIDE CONCENTRATIONS IN RAINWATER WITH A FLOW-INJECTION SYSTEM [J].
FUCSKO, J ;
TOTH, K ;
PUNGOR, E ;
KUNOVITS, J ;
PUXBAUM, H .
ANALYTICA CHIMICA ACTA, 1987, 194 :163-170
[6]  
KARLBERG B., 1989, FLOW INJECTION ANAL, V10
[7]   KINETIC TREATMENT OF UNSEGMENTED FLOW SYSTEMS .3. FLOW-INJECTION SYSTEM WITH GRADIENT CHAMBER EVALUATED WITH A LINEARLY RESPONDING DETECTOR [J].
PARDUE, HL ;
JAGER, P .
ANALYTICA CHIMICA ACTA, 1986, 179 :169-179
[8]   THE USE OF ION-SELECTIVE ELECTRODES IN MANUAL AND COMPUTER-CONTROLLED FLOW-INJECTION SYSTEMS [J].
SLANINA, J ;
LINGERAK, WA ;
BAKKER, F .
ANALYTICA CHIMICA ACTA, 1980, 117 (JUN) :91-98
[9]   Flow-injection analysis wit potentiometric detection for the speciation of fluoride and calcium [J].
Trojanowicz, M ;
Alexander, PW ;
Hibbert, DB .
ANALYTICA CHIMICA ACTA, 1998, 366 (1-3) :23-33
[10]   AN INTEGRATED GRADIENT CHAMBER AND POTENTIOMETRIC DETECTOR FOR FLOW-INJECTION ANALYSIS .2. MEASUREMENT OF ACIDITY CONSTANTS OF WEAK ACIDS [J].
TURNER, DR ;
KNOX, S ;
WHITFIELD, M ;
DOSSANTOS, M ;
PESCADA, C ;
GONCALVES, MD .
ANALYTICA CHIMICA ACTA, 1989, 226 (02) :239-246