Anatase TiO2 porous thin films prepared by sol-gel method using CTAB surfactant

被引:69
作者
Liu, G. Q. [1 ]
Jin, Z. G. [1 ]
Liu, X. X. [1 ]
Wang, T. [1 ]
Liu, Z. F. [1 ]
机构
[1] Tianjin Univ, Sch Mat, Key Lab Adv Ceram & Machining, Minist Educ, Tianjin 300072, Peoples R China
关键词
TiO2 porous thin films; CTAB; sol-gel; phase separation;
D O I
10.1007/s10971-006-0122-9
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Anatase TiO2 porous thin films were prepared on glass substrates by sol-gel method with Cetyltrimethylammonium Bromide (CTAB) as a pore-forming agent, Tetrabutylorthotitanate as Ti precursor, ethanol as solvent and diethanolamine as chelating agent respectively. IR, TG-DSC, XRD and SEM analyzed the chemical and physical changes during sol-gel process and characteristics of the films. Effects of the amount of CTAB, alkane and water on morphology of the films were discussed and the principle of forming porous structure was proposed. It was shown that the diameter of pores was changed in the range of 30-400 nm.
引用
收藏
页码:49 / 55
页数:7
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