Possibilities of gas chromatography atomic emission detection in pesticide multiresidue analysis - Application to herbicide analysis in soils

被引：21

作者：

Bernal, JL

delNozal, MJ

Martin, MT

Jimenez, JJ

机构：

[1] Deparment of Analytical Chemistry, Faculty of Sciences, University of Valladolid, 47005 Valladolid, Prado de la Magdalena s/n

来源：

JOURNAL OF CHROMATOGRAPHY A | 1996年 / 754卷 / 1-2期

关键词：

environmental analysis; detection; GC; soil; pesticides;

D O I：

10.1016/S0021-9673(96)00200-2

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The potential of gas chromatography with atomic emission detection (GC-AED) for pesticide multiresidue analysis is explored. Retention data of 181 phytochemicals of diverse properties and considerations about the identification reliability and sensitivity are provided, making a comparison with data obtained by mass spectrometric (MS) detection. The GC-AED system is applied to the determination of 11 herbicides in laboratory-spiked soils after extraction with ethyl acetate. Complementary use of MS is required in order to resolve some peak pairs undiscerned by AED.

引用

页码：245 / 256

页数：12

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