Microwave assisted preparation of binary oxide nanoparticles

被引：117

作者：

Palchik, O

Zhu, JJ

Gedanken, A ^{[1
]}

机构：

[1] Bar Ilan Univ, Dept Chem, IL-52900 Ramat Gan, Israel

[2] Nanjing Univ, Dept Chem, Nanjing 210093, Peoples R China

来源：

JOURNAL OF MATERIALS CHEMISTRY | 2000年 / 10卷 / 05期

关键词：

D O I：

10.1039/a908795h

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A group of binary oxide nanophase materials were prepared using a microwave assisted soft-chemical route. BaTiO3, Ba6Ti17O40, BaZrO3 and PbTiO3 were prepared from BaCl2 hydrate, Pb(Ac)(2), Ti(OPri)(4) and ZrOCl2. All reactions were performed in ethylene glycol, which acted as both a solvent and a growth regulating agent, under atmospheric pressure in a microwave reactor. The products that were obtained were analyzed by using XRD, TEM, XPS, EDX and FT-IR.

引用

页码：1251 / 1254

页数：4

共 18 条

[1] Characterization of submicron particles of tetragonal BaTiO3 [J].