Solvothermal synthesis to NiE2 (E = Se, Te) nanorods at low temperature

被引：24

作者：

Li, B

Xie, Y ^{[1
]}

Huang, JX

Su, HL

Qian, Y

机构：

[1] Univ Sci & Technol China, Struct Res Lab, Hefei 230026, Anhui, Peoples R China

[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

[3] Univ Sci & Technol China, Dept Phys Chem, Hefei 230026, Anhui, Peoples R China

来源：

NANOSTRUCTURED MATERIALS | 1999年 / 11卷 / 08期

关键词：

D O I：

10.1016/S0965-9773(99)00395-5

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

NiE2 (E = Se, Te) nanorods were directly synthesized through the reaction of NiCl2, and selenium or tellurium in an autoclave at 160 similar to 180 degrees C for 10 similar to 15 h, using ethylenediamine as a solvent. X-ray powder diffraction patterns and transmission electron microscope images show that the products are cubic NiSe2 and hexagonal NiTe2 phase, respectively, in the form of well-crystallized nanorods. A possible mechanism of;he formation of NiE2 nanorods in the solvothermal process is proposed. The solvent ethylenediamine plays an important role in the formation of NiE2 nanorods. (C) 2000 Acta Metallurgica Inc.

引用

页码：1067 / 1071

页数：5

共 28 条

[1] ON TELLURIDES OF NICKEL [J].