Improvements of a combined size exclusion chromatography and solid phase extraction approach for the clean-up of marine sediment samples for trace analysis of pesticides

被引:16
作者
Bester, K
Huhnerfuss, H
机构
[1] Institut für Organische Chemie, D-20146 Hamburg
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1997年 / 358卷 / 05期
关键词
D O I
10.1007/s002160050481
中图分类号
O65 [分析化学];
学科分类号
070302 [分析化学]; 081704 [应用化学];
摘要
Two methods based on gel permeation chromatography (GPC) [size exclusion chromatography] for the analysis of traces (ng/kg) of nitrogen and phosphorus containing pesticides (like triazines or phosphothionates) from marine sediment samples are compared: A macro GPC with Biobeads SX-3 and a chromatography on a high-performance (HP-GPC) column with UV-detection. Results for eight triazine herbicides, two triazine metabolites. the phenylurea derivative linuron, two acetanilides and two organophosphorus compounds are given. Concentrations obtained with the HP-GPC are compared with those obtained with a macro GPC approach in an earlier study.
引用
收藏
页码:630 / 634
页数:5
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