Three minimum wet thickness regions of slot die coating

被引:79
作者
Chang, Yu-Rong
Chang, Hsien-Ming
Lin, Chi-Feng
Liu, Ta-Jo [1 ]
Wu, Ping-Yao
机构
[1] Natl Tsing Hua Univ, Dept Chem Engn, Hsinchu 300, Taiwan
[2] Ind Technol & Res Inst, Mat & Chem Lab, Chutong 300, Taiwan
关键词
slot die coating; minimum wet thickness; capillary number; Reynolds number; flow visualization; static and dynamic contact angles;
D O I
10.1016/j.jcis.2006.11.054
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
An experimental study was carried out to determine the minimum wet thickness of slot die coating for low-viscosity solutions. There exist three distinct coating regions (I, II, and III), depending on the physical properties of the coating fluid, die geometry, and flow conditions. A critical Reynolds number was found, below which viscous and surface tension effects are important. In Region I, the minimum wet thickness increases with increasing capillary number and becomes independent of capillary number in Region II. Region III exists above the critical Reynolds number where fluid inertia is dominant. In this region, the minimum wet thickness decreases as Reynolds number increases. Flow visualization on the coating bead reveals that the position of the downstream meniscus of the coating bead determines the types of coating region, whereas the shape and position of the upstream meniscus determine the type of coating defects. It was also observed that the downstream meniscus was not located at the die lip corner and both the static and dynamic contact angles varied under different conditions. These findings are critical for realistic theoretical study of slot die coating (c) 2006 Elsevier Inc. All rights reserved.
引用
收藏
页码:222 / 230
页数:9
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