Two methods for the resolution of 10,10′-dihydroxy-9,9′-biphenanthryl

被引：8

作者：

Lin, YH

Chien, LC ^{[1
]}

机构：

[1] Kent State Univ, Inst Liquid Crystal, Kent, OH 44242 USA

[2] Kent State Univ, NSF, ALCOM Ctr, Kent, OH 44242 USA

来源：

TETRAHEDRON-ASYMMETRY | 1998年 / 9卷 / 01期

关键词：

D O I：

10.1016/S0957-4166(97)00618-6

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two methods for the resolution of 10,10'-dihydroxy-9,9'-biphenanthryl were developed. The first involved salt formation with (-)-strychnine via its cyclic diester with phosphoric acid. The second method involved the formation of diastereomers (R)- and (S)-9,9'-biphenanthryl-10,10'-diyl N-((-)-alpha-methylbenzyl)phosphoroamidates. (C) 1998 Elsevier Science Ltd. All rights reserved.

引用

页码：63 / 70

页数：8

共 11 条

[1] A NEW AND EFFICIENT METHOD FOR THE RESOLUTION OF 1,1'-BINAPHTHALENE-2,2'-DIOL
BRUNEL, JM
BUONO, G
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1993, 58 (25) : 7313 - 7314
[2] CHIEN LC, 1997, POLYM PREPRINTS, V38, P359
[3] PREPARATION OF ENANTIOMERICALLY PURE 1,1'-BINAPHTHALENE-2,2'-DIOL AND 1,1'-BINAPHTHALENE-2,2'-DITHIOL
FABBRI, D
DELOGU, G
DELUCCHI, O
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1993, 58 (07) : 1748 - 1750
[4] A NEW AND EFFICIENT METHOD FOR THE RESOLUTION OF 2,2'-DIHYDROXY-1,1'-BINAPHTHYL
GONG, BQ
CHEN, WY
HU, BF
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1991, 56 (01) : 423 - 425
[5] HU QS, 1995, TETRAHEDRON-ASYMMETR, V6, P2123
[6] JACQUES J, 1988, ORG SYNTH, V67, P1
[7] A CONVENIENT PREPARATION OF OPTICALLY-ACTIVE 1,1'-BINAPHTHYL-2,2'-DIOL VIA ENZYMATIC-HYDROLYSIS OF THE RACEMIC DIESTER
MIYANO, S
KAWAHARA, K
INOUE, Y
HASHIMOTO, H
[J]. CHEMISTRY LETTERS, 1987, (02) : 355 - 356
[8] ROSINI C, 1992, SYNTHESIS-STUTTGART, P503
[9] TAMAI T, 1990, SYNTHESIS-STUTTGART, P222
[10] OPTICAL RESOLUTION OF BINAPHTHYL AND BIPHENANTHRYL DIOLS BY INCLUSION CRYSTALLIZATION WITH N-ALKYLCINCHONIDIUM HALIDES - STRUCTURAL CHARACTERIZATION OF THE RESOLVED MATERIALS
TODA, F
TANAKA, K
STEIN, Z
GOLDBERG, I
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1994, 59 (19) : 5748 - 5751

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