Preparation of Ag2S nanocrystals of predictable shape and size

被引:152
作者
Lim, WP
Zhang, Z
Low, HY
Chin, WS
机构
[1] Natl Univ Singapore, Dept Chem, Singapore 117543, Singapore
[2] Inst Mat Res & Engn, Singapore 117602, Singapore
关键词
chalcogenides; crystal growth; electron microscopy; nanostructures;
D O I
10.1002/anie.200460566
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In control! Ag2S nanocrystals of predictable size and shape were synthesized from the precursor Ag(SCOPh) in the presence of an amine. Careful tuning of several parameters, such as the reaction temperature and the ratio of amine to precursor, led to Ag2S nanocrystals of varying morphology (red: nanocubes; blue: faceted nanocrystals; yellow: nanorods) and size, x = particle size. HDA = hexadecylamine.
引用
收藏
页码:5685 / 5689
页数:5
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