A multi-residue screening method for the determination of 73 pesticides and metabolites in fruit and vegetables using high-performance liquid chromatography/tandem mass spectrometry

被引：65

作者：

Hetherton, CL

Sykes, MD ^{[1
]}

Fussell, RJ

Goodall, DM

机构：

[1] Cent Sci Lab, York YO41 1LZ, N Yorkshire, England

[2] Univ York, Dept Chem, York YO10 5DD, N Yorkshire, England

来源：

RAPID COMMUNICATIONS IN MASS SPECTROMETRY | 2004年 / 18卷 / 20期

关键词：

D O I：

10.1002/rcm.1645

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A multi-residue screening method was developed for the simultaneous analysis of 73 pesticides and their metabolites using high-performance liquid chromatography coupled with electrospray tandem mass spectrometry. These pesticides were determined under a single set of experimental conditions involving a simple acetonitrile extraction without the requirement for a clean-up step. Validation was achieved at 0.01 and 0.1 mg kg(-1) levels in apple, lettuce and orange. Recoveries were in the range 77-124% for the majority of pesticides. (C) Crown Copyright 2004. Reproduced with the permission of Her Majesty's Stationery Office. Published by John Wiley Sons, Ltd.

引用

页码：2443 / 2450

页数：8

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