Silicon carbide powder synthesis by chemical vapour deposition from silane/acetylene reaction system

被引:38
作者
Kavecky, S
Janeková, B
Madejová, J
Sajgalík, P
机构
[1] Slovak Acad Sci, Inst Mat & Machine Mech, SK-83812 Bratislava, Slovakia
[2] Slovak Acad Sci, Inst Inorgan Chem, SK-84236 Bratislava, Slovakia
关键词
chemical properties; CVD; grain size; powders; SiC;
D O I
10.1016/S0955-2219(00)00071-6
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Amorphous fine silicon carbide powders have been prepared via the chemical vapour deposition from reaction mixture SiH4-C2H2 in a vertical tubular flow reactor in the temperature range 900-1250 degrees C. Powder particles prepared at temperature 1100 degrees C and C2H2/SiH4 mol ratio 1.2 are equiaxial, quasispherical and agglomerated. The mean particle size of the powder is approx. 0.1-0.2 mu m. The maximum agglomerate size is about 0.3 mu m. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:1939 / 1946
页数:8
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