Purification of single-walled carbon nanotubes synthesized by the catalytic decomposition of hydrocarbons

被引:69
作者
Li, F
Cheng, HM [1 ]
Xing, YT
Tan, PH
Su, G
机构
[1] Chinese Acad Sci, Inst Met Res, Shenyang 110015, Peoples R China
[2] Chinese Acad Sci, Inst Semicond, Natl Lab Superlattices & Microstruct, Beijing 100083, Peoples R China
基金
中国国家自然科学基金;
关键词
carbon nanotubes; chemical treatment;
D O I
10.1016/S0008-6223(00)00061-0
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A procedure for purifying single-walled carbon nanotubes (SWNTs) synthesized by the catalytic decomposition of hydrocarbons has been developed. Based on the results from SEM observations, EDS analysis and Raman measurements, it was found that amorphous carbon, catalyst particles, vapor-grown carbon nanofibers and multi-walled carbon nanotubes were removed from the ropes of SWNTs without damaging the SWNT bundles, and a 40% yield of the SWNTs with a purity of about 95% was achieved after purification. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:2041 / 2045
页数:5
相关论文
共 10 条
  • [1] Intercalation and partial exfoliation of single-walled carbon nanotubes by nitric acid
    Bower, C
    Kleinhammes, A
    Wu, Y
    Zhou, O
    [J]. CHEMICAL PHYSICS LETTERS, 1998, 288 (2-4) : 481 - 486
  • [2] Large-scale and low-cost synthesis of single-walled carbon nanotubes by the catalytic pyrolysis of hydrocarbons
    Cheng, HM
    Li, F
    Su, G
    Pan, HY
    He, LL
    Sun, X
    Dresselhaus, MS
    [J]. APPLIED PHYSICS LETTERS, 1998, 72 (25) : 3282 - 3284
  • [3] PYROLYTIC CARBON NANOTUBES FROM VAPOR-GROWN CARBON-FIBERS
    ENDO, M
    TAKEUCHI, K
    KOBORI, K
    TAKAHASHI, K
    KROTO, HW
    SARKAR, A
    [J]. CARBON, 1995, 33 (07) : 873 - 881
  • [4] Large-scale production of single-walled carbon nanotubes by the electric-arc technique
    Journet, C
    Maser, WK
    Bernier, P
    Loiseau, A
    delaChapelle, ML
    Lefrant, S
    Deniard, P
    Lee, R
    Fischer, JE
    [J]. NATURE, 1997, 388 (6644) : 756 - 758
  • [5] LI F, 1998, INT S CARB TOK JAP C, V98, P548
  • [6] Diameter-selective Raman scattering from vibrational modes in carbon nanotubes
    Rao, AM
    Richter, E
    Bandow, S
    Chase, B
    Eklund, PC
    Williams, KA
    Fang, S
    Subbaswamy, KR
    Menon, M
    Thess, A
    Smalley, RE
    Dresselhaus, G
    Dresselhaus, MS
    [J]. SCIENCE, 1997, 275 (5297) : 187 - 191
  • [7] Purification of single-wall carbon nanotubes by ultrasonically assisted filtration
    Shelimov, KB
    Esenaliev, RO
    Rinzler, AG
    Huffman, CB
    Smalley, RE
    [J]. CHEMICAL PHYSICS LETTERS, 1998, 282 (5-6) : 429 - 434
  • [8] Crystalline ropes of metallic carbon nanotubes
    Thess, A
    Lee, R
    Nikolaev, P
    Dai, HJ
    Petit, P
    Robert, J
    Xu, CH
    Lee, YH
    Kim, SG
    Rinzler, AG
    Colbert, DT
    Scuseria, GE
    Tomanek, D
    Fischer, JE
    Smalley, RE
    [J]. SCIENCE, 1996, 273 (5274) : 483 - 487
  • [9] Purifying single-walled nanotubes
    Tohji, K
    Goto, T
    Takahashi, H
    Shinoda, Y
    Shimizu, N
    Jeyadevan, B
    Matsuoka, I
    Saito, Y
    Kasuya, A
    Ohsuna, T
    Hiraga, H
    Nishina, Y
    [J]. NATURE, 1996, 383 (6602) : 679 - 679
  • [10] Purification procedure for single-walled nanotubes
    Tohji, K
    Takahashi, H
    Shinoda, Y
    Shimizu, N
    Jeyadevan, B
    Matsuoka, I
    Saito, Y
    Kasuya, A
    Ito, S
    Nishina, Y
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 1997, 101 (11): : 1974 - 1978