Structural and magnetic properties of carbonyl Fe-Ni nanometer particles

被引:21
作者
Ge, FD [1 ]
Chen, LM [1 ]
Ku, WJ [1 ]
Zhu, J [1 ]
机构
[1] TSING HUA UNIV,DEPT MAT SCI & ENGN,BEIJING 100084,PEOPLES R CHINA
来源
NANOSTRUCTURED MATERIALS | 1997年 / 8卷 / 06期
关键词
D O I
10.1016/S0965-9773(97)00217-1
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The phases, size, shape, aggregation pattern and chemical composition of carbonyl Fe-Ni ultrafine particles prepared by thermal decomposition of the mixture of Fe(CO)(5) and M(CO)(4) were investigated by X-ray diffraction and electron microscopy. It was found that the main phase was gamma-(Fe-Ni), including a small amount of Fe3O4. The particle size was about 10 nm and the particles formed a fractal aggregation pattern whose dimension was 1.64. The composition varied from particle to particle, showing an average value of Fe44Ni56. The magnetic properties of the particles were examined with a vibrating sample magnetometer. (C) 1997 Acta Metallurgica Inc.
引用
收藏
页码:703 / 709
页数:7
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