Investigations on the product distribution pattern during the electrochemical fluorination of 2-fluoropyridine and pyridine

被引：12

作者：

Sartori, P

Velayutham, D

Ignat'ev, N

Noel, M

机构：

[1] Gerhard Mercator Univ, D-47057 Duisburg, Germany

[2] CSIR, Cent Electrochem Res Inst, Karaikudi 630006, Tamil Nadu, India

来源：

JOURNAL OF FLUORINE CHEMISTRY | 1998年 / 87卷 / 01期

关键词：

electrochemical fluorination; 2-fluoropyridine; pyridine; perfluoropiperidine;

D O I：

10.1016/S0022-1139(97)00095-X

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

By using 2-fluoropyridine instead of pyridine as the starting material, a 19% conversion yield of perfluoropiperidine was obtained during the electrochemical fluorination process. At least ten products including perfluoropiperidine were characterised using repeated fractional distillation followed by GC and NMR analysis. (C) 1998 Elsevier Science S.A.

引用

页码：31 / 36

页数：6

共 16 条

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