Large scale synthesis of dysprosium and neodymium diiodides

被引:40
作者
Evans, WJ [1 ]
Allen, NT [1 ]
Workman, PS [1 ]
Meyer, JC [1 ]
机构
[1] Univ Calif Irvine, Dept Chem, Irvine, CA 92697 USA
关键词
D O I
10.1021/ic0300316
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
DyI2 and NdI2, which may become useful reagents in organic synthesis, can be prepared in up to 50 g quantities in a few hours without using welded tantalum tubes or temperatures over 1000 degreesC by direct reaction of the metal and iodine.
引用
收藏
页码:3097 / 3099
页数:3
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