Synthesis of SnO and SnO2 nanocrystalline powders by the gas phase condensation method

被引：34

作者：

Jimenez, VM

GonzalezElipe, AR

Espinos, JP

Justo, A

Fernandez, A

机构：

[1] INST CIENCIA MAT SEVILLA,E-41080 SEVILLE,SPAIN

[2] DEPT QUIM INORGAN,E-41080 SEVILLE,SPAIN

来源：

SENSORS AND ACTUATORS B-CHEMICAL | 1996年 / 31卷 / 1-2期

关键词：

gas phase condensation; nanostructured tin oxides;

D O I：

10.1016/0925-4005(96)80012-8

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The present paper deals with the study of the application of the gas phase condensation method to the synthesis of nanostructured tin oxides (SnO and SnO2). The method consists of the evaporation of a precursor compound (Sn, SnO, SnO2) in an inert gas atmosphere (He) to collect an ultrafine powder. The analysis of the obtained materials by XRD (X-ray diffraction), TEM (transmission electron microscopy) and XPS (X-ray photoelectron spectroscopy) allows us to determine the experimental conditions that produce the best nanostructured ultrafine powders.

引用

页码：29 / 32

页数：4

共 21 条

[1]

BALZERS, 1991, COATINGS MATERIALS S

[2]

BRATTAIN WH, 1953, AT&T TECH J, V32, P1

[3]

Eastman J. A., 1992, Nanostructured Materials, V1, P47, DOI 10.1016/0965-9773(92)90051-X

[4] Magnetism of ultrafine particles [J].

Gangopadhyay, S. ;

Hadjipanayis, G.C. ;

Dale, B. ;

Sorensen, C.M. ;

Klabunde, K.J. .

Nanostructured Materials, 1992, 1 (01)

[5] NANOCRYSTALLINE MATERIALS [J].

BIRRINGER, R .

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 1989, 117 :33-43

[6] NANOSTRUCTURED MATERIALS [J].

GLEITER, H .

ADVANCED MATERIALS, 1992, 4 (7-8) :474-481

[7]

Gleiter H., 1992, Nanostructured Materials, V1, P1, DOI 10.1016/0965-9773(92)90045-Y

[8] Ultrafine oxide powders prepared by inert gas evaporation [J].

Gunther, B. ;

Kumpmann, A. .

Nanostructured Materials, 1992, 1 (01)

[9]

HAGEN W, 1983, ADV SOLID STATE PHYS, V23, P259

[10] ZUM EINFLUSS VON ADSORBIERTEM SAUERSTOFF AUF DIE ELEKTRISCHE LEITFAHIGKEIT VON ZINKOXYDKRISTALLEN [J].

HEILAND, G .

ZEITSCHRIFT FUR PHYSIK, 1954, 138 (3-4) :459-464

← 1 2 3 →