Synthesis and characterization of tin oxide microfibres electrospun from a simple precursor solution

被引:33
作者
Wang, Y
Aponte, M
Leon, N
Ramos, I
Furlan, R
Evoy, S
Santiago-Avilés, JJ
机构
[1] Univ Puerto Rico Humacao, Dept Phys & Elect, CUH Stn, Humacao, PR 00791 USA
[2] Univ Penn, Dept Elect & Syst Engn, Philadelphia, PA 19104 USA
关键词
D O I
10.1088/0268-1242/19/8/017
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Tin oxide (SnO2) microfibres in the rutile structure were synthesized using electrospinning and metallorganic decomposition techniques. Fibres were electrospun from a precursor solution containing 20 mg poly(ethylene oxide) (molecular weight 900 000), 2 ml chloroform and 1 ml dimethyldineodecanoate tin, and sintered in the air for 2 h at 400, 600 and 800degreesC, respectively. Scanning electron microscopy, x-ray diffraction and Raman microspectrometry were used to characterize the sintered fibres. The results showed that the synthesized fibres are composed of SnO2.
引用
收藏
页码:1057 / 1060
页数:4
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