An efficient one-pot procedure for preparation of 2,4(1H,3H)-qninazolinediones and 2-thioxoquinazolinone derivatives under microwave irradiation

被引：50

作者：

Azizian, J ^{[1
]}

Mohammadi, AA ^{[1
]}

Karimi, AR ^{[1
]}

机构：

[1] Shahid Beheshti Univ, Fac Sci, Dept Chem, Tehran, Iran

来源：

SYNTHETIC COMMUNICATIONS | 2003年 / 33卷 / 03期

关键词：

D O I：

10.1081/SCC-120015771

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

An efficient one-pot synthesis of 2,4(1H,3H)-quinazolinediones and 2-thioxoquinazolinone derivatives are given by the condensation of isatoic anhydride, primary amine and urea or thiourea in the absence of organic or inorganic reagents under microwave irradiation.

引用

页码：415 / 420

页数：6

共 19 条

[1] ALTAMANY EH, 1997, EGYPT J CHEM, V40, P339
[2] Microwave-induced one-pot synthesis of some new spiro[3H-indole-3,5′(4′H)-[1,2,4]-triazoline]-2-ones
Azizian, J
Soozangarzadeh, S
Jadidi, K
[J]. SYNTHETIC COMMUNICATIONS, 2001, 31 (07) : 1069 - 1073
[3] Rearrangement of 4-imino-(1H,4H)-3,1-benzoxazine-2-ones to 2,4-quinazolinediones via an isocyanate carboxamide intermediate
Azizian, J
Mehrdad, M
Jadidi, K
Sarrafi, Y
[J]. TETRAHEDRON LETTERS, 2000, 41 (27) : 5265 - 5268
[4] Azizian J., 2001, SYNTHETIC COMMUN, V31, P1
[5] AZIZIAN J, IN PRESS SYNTH COMMU
[6] SYNTHESES OF METEROCYCLES .89. REACTIONS OF ISATOIC ANHYDRIDE WITH DERIVATIVES OF UREA AND THIOUREA
KAPPE, T
STEIGER, W
ZIEGLER, E
[J]. MONATSHEFTE FUR CHEMIE, 1967, 98 (01): : 214 - &
[7] MOLECULAR REARRANGEMENT IN POLYPHOSPHORIC ACID .2. CONVERSION OF 1,2-DIHYDRO-2-PHENYLIMINO-4H-3, 1-BENZOXAZIN-4-ONE TO 3-PHENYL-2,4(1H 3H)-QUINAZOLINEDIONE
KURIHARA, M
YODA, N
[J]. BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1966, 39 (09) : 1942 - +
[8] MEER RKV, 1984, J ORG CHEM, V49, P3373
[9] SYNTHESIS OF 2,4[1H,3H]QUINAZOLINEDIONE AND SOME OF ITS 3-ARYL SUBSTITUTED DERIVATIVES
MICHMAN, M
PATAI, S
WIESEL, Y
[J]. ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1978, 10 (01) : 13 - 16
[10] HETEROCYCLIC SYNTHESIS VIA A TANDEM AZA-WITTIG REACTION HETEROCUMULENE-MEDIATED ANNULATION REACTION - NEW METHODOLOGY FOR THE PREPARATION OF QUINAZOLINE DERIVATIVES
MOLINA, P
ALAJARIN, M
VIDAL, A
[J]. TETRAHEDRON LETTERS, 1988, 29 (31) : 3849 - 3852

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