Abnormal grain growth and grain boundary faceting in a model Ni-base superalloy

Normal or abnormal grain growth in a model Ni-base superalloy is observed to depend on the grain boundary structure when heat-treated in a solid solution temperature range above the solvus temperature (1150 degrees C) of the gamma' phase. When heat-treated at 1200 degrees C abnormal grain growth occurs and most of the grain boundaries are observed to be faceted by optical microscopy, transmission electron microscopy, and scanning electron microscopy at the intergranular fracture surface. Some of the grain boundary facet planes are expected to be singular corresponding to the cusps in the polar plot of the boundary energy against the inclination angle, and it is proposed that if these boundary segments move by a boundary step mechanism, the abnormal grain growth can occur. When heat-treated at 1300 degrees C normal grain growth occurs, the grain boundaries are defaceted, and hence atomically rough. Normal growth is expected if the migration rate of the rough grain boundaries increases linearly with the driving force arising from the grain size difference. The correlation between the grain boundary structural transition and the growth behavior thus appears to be general in pure metals and solid solution alloys. (C) 2000 Acta Metallurgica Inc. Published by Elsevier Science Lid. All rights reserved.