A comparative study of cadmium, lead, mercury, arsenic, selenium, manganese, copper and zinc in brown rice and fish by inductively coupled plasma-mass spectrometry (ICP-MS) and atomic absorption spectrometry

被引：5

作者：

Oshima, H ^{[1
]}

Ueno, E ^{[1
]}

Saito, I ^{[1
]}

Matsumoto, H ^{[1
]}

机构：

[1] Aichi Prefectural Inst Publ Hlth, Kita Ku, Nagoya, Aichi 4628576, Japan

来源：

JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN | 2004年 / 45卷 / 05期

关键词：

ICP-MS; multielemental analysis; brown rice; fish; atomic absorption spectrometry;

D O I：

10.3358/shokueishi.45.270

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

A study was conducted to evaluate the applicability of ICP-MS techniques for determination of metals in brown rice and fish. Cadmium, lead, mercury, arsenic, selenium, manganese, copper and zinc were determined by this method. An open digestion with nitric acid (Method A) and a rapid open digestion with nitric acid and hydrochloric acid (Method B) were used to solubilize analytes in samples, and these procedures were followed by ICP-MS analysis. Recovery of certified elements from standard reference materials by Method A and Method B ranged from 92 to 110% except for mercury (70 to 100%). Analytical results of brown rice and fish samples obtained by this ICP-MS agreed with those obtained by atomic absorption spectrometry (AAS). The results of this study demonstrate that quadrupole ICP-MS provides precise and accurate measurements of the elements tested in brown rice and fish samples.

引用

页码：270 / 276

页数：7

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