Growth of columnar aluminum nitride layers on Si(111) by molecular beam epitaxy

被引:32
作者
Karmann, S [1 ]
Schenk, HPD [1 ]
Kaiser, U [1 ]
Fissel, A [1 ]
Richter, W [1 ]
机构
[1] Univ Jena, Inst Festkorperphys, D-07743 Jena, Germany
来源
MATERIALS SCIENCE AND ENGINEERING B-SOLID STATE MATERIALS FOR ADVANCED TECHNOLOGY | 1997年 / 50卷 / 1-3期
关键词
AlN; film; Si(111)-substrate; MBE; TEM;
D O I
10.1016/S0921-5107(97)00168-2
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Single crystalline aluminum nitride (AlN) thin films are deposited by molecular bt am epitaxy (MBE) using thermally evaporated aluminum and RF-plasma excited nitrogen gas. In this paper we report on films grown on Si(111) at substrate temperatures of 800 degrees with growth rates between 65 and 350 nm h(-1). All layers consist of hexagonal and exactly c-axis oriented AlN crystals with column-like structure. For the smoothest layers surface roughness (rms) around 1 nm is obtained. In the XRD-spectra (omega-scan) we have achieved a minimum FWHM of 0.4 degrees (=25') for the AlN(00.2) reflex. At maximum growth rates (350 nm h(-1)) ibr AlN a transition zone of about 200 nm is formed with high defect density compared to the subsequent growth. For lower growth rates (65 nm h(-1)) no transition zone exists. Application of a substrate nitridation leads to a partial loss of epitaxial relation between AIN layer and Si(111)-substrate. (C) 1997 Elsevier Science S.A.
引用
收藏
页码:228 / 232
页数:5
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