Development of porous and dispersed CRM

被引:2
作者
Rohl-Kuhn, B [1 ]
Meyer, K [1 ]
Klobes, P [1 ]
Fritz, T [1 ]
机构
[1] Fed Inst Mat Res & Testing BAM, D-12200 Berlin, Germany
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1998年 / 360卷 / 3-4期
关键词
SiO2; Pore Volume; Meso; Certify Reference Material; Classification Type;
D O I
10.1007/s002160050720
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Porous and finely dispersed certified reference materials (CRM) were certified using the gas adsorption method. The special certification procedure for IUPAC isotherm classification types I, IT, and IV is presented for meso- and macroporous materials with special emphasis on specific surface area, specific pore volume and pore width according to standards DIN 66 131, 66 134, and 66 135. Four CRMs (SiO2, alpha-Al2O3, two transition aluminas) with a macro-and mesopore range are presented. Certification was made on the basis of BCR guidelines in connection with interlaboratory tests (altogether 38 participating laboratories, 44 various gas adsorption apparatus).
引用
收藏
页码:393 / 397
页数:5
相关论文
共 12 条
[1]  
Avnir D., 1989, The Fractal Approach to Heterogeneous Chemistry: Surfaces, Colloids, Polymers
[2]  
*BCR, 1994, BCR4893
[3]  
*DIN, 1993, 66131 DIN BET
[4]  
*DIN, 1995, 66134 DIN BJH
[5]  
*DIN ISO, 1988, 5725 DINISO
[6]  
GREGG SJ, 1982, ADSORPTION SURFACE
[7]  
*MEAS TEST PROGR E, SMT4CT952025 MEAS TE
[8]   POROUS SOLIDS AND THEIR CHARACTERIZATION - METHODS OF INVESTIGATION AND APPLICATION [J].
MEYER, K ;
LORENZ, P ;
BOHLKUHN, B ;
KLOBES, P .
CRYSTAL RESEARCH AND TECHNOLOGY, 1994, 29 (07) :903-930
[9]  
Patrick J.W., 1995, POROSITY CARBONS CHA
[10]  
ROHLKUHN B, 1997, IN PRESS CHARACTERIZ, V4