71Ga and 31P solid state NMR:: a powerful tool for the characterization of the first gallium phosphonates

被引:44
作者
Fredoueil, F
Massiot, D
Poojary, D
Bujoli-Doeuff, M
Clearfield, A
Bujoli, B
机构
[1] UMR CNRS 6513, Organ Synth Lab, F-44322 Nantes 03, France
[2] Ctr Rech Phys Hautes Temp, UPR CNRS 4212, F-45071 Orleans, France
[3] Texas A&M Univ, Dept Chem, College Stn, TX 77843 USA
[4] UMR CNRS 6502, Inst Mat Nantes, F-44322 Nantes 03, France
关键词
D O I
10.1039/a705270g
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Two new gallium phosphonates Ga(OH)(O3PC2H4CO2H) . H2O 1 and Ga-3(OH)(3)(O3PC2H4CO2)(2) . 2H(2)O 2 are prepared and characterized, using P-31 MAS and Ga-71 static NMR spectroscopy, showing a good correspondence between the fitted NMR parameters and the crystallographic data.
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收藏
页码:175 / 176
页数:2
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