Characterization of binary gold/platinum nanoparticles prepared by sonochemistry technique

被引:38
作者
Nakanishi, M
Takatani, H
Kobayashi, Y
Hori, F
Taniguchi, R
Iwase, A
Oshima, R
机构
[1] Osaka Prefecture Univ, Adv Sci & Technol Res Inst, Sakai, Osaka 5998570, Japan
[2] Kyoto Univ, Inst Res Reactor, Osaka 5900494, Japan
关键词
sonochemistry; gold-platinum alloy; nanoparticle; core-shell structure; HRTEM; Au-197 Mossbauer spectroscopy;
D O I
10.1016/j.apsusc.2004.09.046
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Aqueous solutions with Au3+ and Pt4+ ions and additives of surfactants (SDS or PEG-MS) were irradiated with an ultrasound 2 at 200 kHz with an input power of 4.2 W/cm(2) and colloidal nanoparticles were prepared. The prepared nanoparticles were characterized by XRD, TEM, HRTEM, EDX and Au-197 Mossbauer spectroscopy. It was found that the structures of nanoparticles were changed with the surfactants; Au and Pt nanoparticles were prepared individually by using SDS, and bimetallic Au/Pt alloy nanoparticles with a core-shell structure were produced in the presence of PEG-MS. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:209 / 212
页数:4
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