Preparation of ultrafine zirconia powder by emulsion method

被引:31
作者
Gao, L
Qiao, HC
Qiu, HB
Yan, DS
机构
[1] Stt. Key Lab. High Perf. Ceramics S., Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050
关键词
D O I
10.1016/0955-2219(95)00115-8
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Ultrafine 14 nm 3 mol% Y2O3 stabilized tetragonal ZrO2 powder was prepared by emulsion processing. The obtained particles were weakly agglomerated into polyhedral or spherical shaped powders. The powder characteristics were investigated by using X-ray diffraction (XRD), X-ray fluoroescence (XRF), inductively coupled plasma spectroscopy (lCP), nitrogen adsorption (BET model) and thermal analysis (DTA-TG). The experiments indicated that the heterogenous distillation used in the process was an effective method to remove residual water in the gel-precipitate and reduce the formation of strong agglomerates. The powder presented good formability and sinterability.
引用
收藏
页码:437 / 440
页数:4
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